User:Matt Hartings/Notebook/Phosphorylation/2012/09/17: Difference between revisions

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==Description==
==Description==
# Add experimental record here. Include what, how, and why...
Following protocol [http://cfs.umbi.umd.edu/cfs/reprints/Long-Lifetime%20Ru(II)%20Complexes%20as%20Labeling.pdf Lackowicz paper]
#1mmol of [Ru(Cl)<sub>2</sub>(bpy)<sub>2</sub>] added to 50mL roundbottom (0.4816g)
#1mmol of 1,10-phenanthroline 5-amine added to 50mL roundbottom (0.1974g)
#25mL of methanol added
#Reaction run under N<sub>2</sub> and refluxed for 3 hours (started at 11 am)


==Data==
==Data==

Revision as of 10:14, 17 September 2012

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Objective

Synthesize new Ru(bpy)2(phen-NH2) for ATP synthesis.

Description

Following protocol Lackowicz paper

  1. 1mmol of [Ru(Cl)2(bpy)2] added to 50mL roundbottom (0.4816g)
  2. 1mmol of 1,10-phenanthroline 5-amine added to 50mL roundbottom (0.1974g)
  3. 25mL of methanol added
  4. Reaction run under N2 and refluxed for 3 hours (started at 11 am)

Data

  • Add data and results here...

Notes

This area is for any observations or conclusions that you would like to note.

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