User:Madeleine Y. Bee/Notebook/Single Molecule Fluorescence/2013/10/09: Difference between revisions
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*Procedure adapted from "On the preparation of metalloporphyrins" | *Procedure adapted from "On the preparation of metalloporphyrins" | ||
**0.5g tetraphenylporphyrin refluxed in 50mL DMF | **0.5g tetraphenylporphyrin refluxed in 50mL DMF | ||
**0.403g (stiochiometric amount) zinc acetate added, solution refluxed | **0.403g (stiochiometric amount) zinc acetate added, solution refluxed until reaction complete | ||
***completion determination by unchanged peaks in UV-vis measurements | |||
**50mL distilled water added, solution chilled and then filtered | **50mL distilled water added, solution chilled and then filtered | ||
***the filtrate was filtered over again and added to main filtered sample | ***the filtrate was filtered over again and added to main filtered sample | ||
===Data=== | ===Data=== | ||
Absorbance Measurements | Absorbance Measurements |
Revision as of 08:25, 16 October 2013
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October 9, 2013Procedures
DataAbsorbance Measurements
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