Difference between revisions of "User:Karlena L. Brown/Notebook/PVOH Research/2013/03/20"

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|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> PVOH Research</span>
 
|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> PVOH Research</span>
|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}}
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|style="background-color: #F2F2F2" align="center"|[[File:Report.png|frameless|link={{#sub:{{FULLPAGENAME}}|0|-11}}]][[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|[[File:Resultset_previous.png|frameless|link={{#lnpreventry:{{FULLPAGENAME}}}}]][[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]][[File:Resultset_next.png|frameless|link={{#lnnextentry:{{FULLPAGENAME}}}}]]}}
 
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* Prepare more microsphere samples expanding upon new previous method developed (new modifications)
 
* Prepare more microsphere samples expanding upon new previous method developed (new modifications)
  
==PVOH 146K & 130K Prepared Microsphere Samples & Dye Preparations 4==
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==PVOH 146K Prepared Microsphere Samples & Dye Preparations 4==
 
'''RECALL MICROSPHERE PREPARATION PROTOCOL ON 2/20/13'''
 
'''RECALL MICROSPHERE PREPARATION PROTOCOL ON 2/20/13'''
  
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| 90:10||110% CEC NaMT w/ DMHXLBR||0.01070||0.09100||40||92||109
 
| 90:10||110% CEC NaMT w/ DMHXLBR||0.01070||0.09100||40||92||109
 
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==PVOH 130K Prepared Microsphere Samples & Dye Preparations==
 +
'''RECALL MICROSPHERE PREPARATION PROTOCOL ON 2/20/13'''
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 +
'''1μM Rhodamine 6G Dye Concentration (90:10)'''
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  M<sub>1</sub>V<sub>1</sub> = M<sub>2</sub>V<sub>2</sub>
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  1μM (RG6)x 10mL = (92μM)V<sub>2</sub>    V<sub>2</sub> = 109μL
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'''1μM Rhodamine 6G Dye Concentration (50:50)'''
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  M<sub>1</sub>V<sub>1</sub> = M<sub>2</sub>V<sub>2</sub>
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  1μM (RG6)x 10mL = (165μM)V<sub>2</sub>    V<sub>2</sub> = 61μL
  
 
{| {{table}}
 
{| {{table}}
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==Notes==
 
==Notes==
* Unfortunately, DSC samples were not taken before the Rhodamine 6G dye was added; therefore, these samples must be remade.
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* Unfortunately, DSC samples were not taken before the Rhodamine 6G dye was added to each sample; therefore, these samples must be remade.
  
 
<!-- ##### DO NOT edit below this line unless you know what you are doing. ##### -->
 
<!-- ##### DO NOT edit below this line unless you know what you are doing. ##### -->

Latest revision as of 21:34, 26 September 2017

Owwnotebook icon.png PVOH Research Report.pngMain project page
Resultset previous.pngPrevious entry      Next entryResultset next.png

OBJECTIVES

  • Continue to clean, filter, and separate out the oil from the previously prepared microspheres on 2/22/13
  • Prepare more microsphere samples expanding upon new previous method developed (new modifications)

PVOH 146K Prepared Microsphere Samples & Dye Preparations 4

RECALL MICROSPHERE PREPARATION PROTOCOL ON 2/20/13

1μM Rhodamine 6G Dye Concentration (90:10)

  M1V1 = M2V2
  1μM (RG6)x 10mL = (92μM)V2    V2 = 109μL

1μM Rhodamine 6G Dye Concentration (50:50)

  M1V1 = M2V2
  1μM (RG6)x 10mL = (165μM)V2    V2 = 61μL
PVOH vs. Clay Ratio Clay Selection PVOH 146K Mass (g) Actual Clay Mass (g) H2O Added (mL) Dye Concentration (μM) Dye Amount Added (μL)
50:50 110% CEC NaMT w/ DMHXLBR 0.05010 0.05100 40 165 61
90:10 110% CEC NaMT w/ DMHXLBR 0.01070 0.09100 40 92 109

PVOH 130K Prepared Microsphere Samples & Dye Preparations

RECALL MICROSPHERE PREPARATION PROTOCOL ON 2/20/13

1μM Rhodamine 6G Dye Concentration (90:10)

  M1V1 = M2V2
  1μM (RG6)x 10mL = (92μM)V2    V2 = 109μL

1μM Rhodamine 6G Dye Concentration (50:50)

  M1V1 = M2V2
  1μM (RG6)x 10mL = (165μM)V2    V2 = 61μL
PVOH vs. Clay Ratio Clay Selection PVOH 130K Mass (g) Actual Clay Mass (g) H2O Added (mL) Dye Concentration (μM) Dye Amount Added (μL)
50:50 110% CEC NaMT w/ DMHXLBR 0.05070 0.05130 40 165 61
90:10 110% CEC NaMT w/ DMHXLBR 0.01090 0.09340 40 92 109

Notes

  • Unfortunately, DSC samples were not taken before the Rhodamine 6G dye was added to each sample; therefore, these samples must be remade.