Difference between revisions of "User:Ellen Petersen/Notebook/MOF Continued/2013/04/02"

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|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> OF: Tara</span>
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|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> MOF: Tara</span>
 
|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}}
 
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* 11.) NMR in Chloroform (See Image Below)
 
* 11.) NMR in Chloroform (See Image Below)
  
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[[Image:040313.png‎|200px|NMR DPNI]]
  
  

Revision as of 11:33, 1 July 2013

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DPNI

  • 1.) Add solids 1,4,5,8 Naphthalenetetracarboxylic dianhydride (.4025 g, 3.00 mmol) and 4-aminopyridine (.4235 g, 6.00 mmol)to round bottom flask
  • 2.) Add 75 mL of solvent (DMA) ~keep under hood~
  • 3.) Add Stir Bar to solution
  • 4.) Put under spout and raise black knob until there is enough pressure to hold it in place
  • 5.) Begin to stir
  • 6.) If attached to condenser, turn on water very slightly
  • 7.) Turn on nitrogen: ensure bubbles are about 1 every 4 seconds. (Turn little end of nossle up)
  • 8.) Turn on heat to 40, switch down accordingly until it reaches 135 degrees consistently.

______________________________________________________________________________________________________

04-03-13

  • 9.) Turn off nitrogen and water, Cool to Room Temperature
  • 10.) Filter out solid using diethyl ether
  • 11.) NMR in Chloroform (See Image Below)

NMR DPNI