Difference between revisions of "User:Ellen Petersen/Notebook/MOF Continued/2013/03/06"

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(Remove amorphous material in PPF-18)
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==Remove amorphous material in PPF-18==
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==Remove amorphous material in PPF-18 & Synthesizing Sheets==
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* 1.) Combine Vials ( EK 2/4/13, EMP 11/16/13, AEM 1/8/13, AEM 1/28/13)
 
* 1.) Combine Vials ( EK 2/4/13, EMP 11/16/13, AEM 1/8/13, AEM 1/28/13)
 
* 2.) Add .0092 g to small vial
 
* 2.) Add .0092 g to small vial
 
* 3.) Add 1.5 mL DEF, .5 mL ethanol, .0175014 g Adenine
 
* 3.) Add 1.5 mL DEF, .5 mL ethanol, .0175014 g Adenine
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*Powder X-Ray Diffraction taken of PPF-18, and PPF-18 with adenine
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[[Image:31313.png‎|200px|PPF-18]]
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[[Image:031313.png‎|200px|PPF-18 with Adenine]]
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[[Image:032713.png‎|200px|PPF-18 with Adenine]]
 
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_________________________________________________________________________________________________________________
 
03-06-13
 
03-06-13
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*5.) Powder X-Ray Diffraction (See Image 1 below)
 
*5.) Powder X-Ray Diffraction (See Image 1 below)
  
[[Image:032013.png‎|200px|Description of image]]
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[[Image:032012.png‎|200px|Sheets]]
  
03-08-13
 
  
* 4.)Filter 
 
 
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Revision as of 05:26, 28 June 2013

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Remove amorphous material in PPF-18 & Synthesizing Sheets

  • 1.) Combine Vials ( EK 2/4/13, EMP 11/16/13, AEM 1/8/13, AEM 1/28/13)
  • 2.) Add .0092 g to small vial
  • 3.) Add 1.5 mL DEF, .5 mL ethanol, .0175014 g Adenine
  • Powder X-Ray Diffraction taken of PPF-18, and PPF-18 with adenine


PPF-18

PPF-18 with Adenine

PPF-18 with Adenine _________________________________________________________________________________________________________________ 03-06-13

  • Synthesizing Sheets:
  • 1.) Add 7.9 mg (0.01 mmol) TCPP, 8.9 (0.03 mmmol) zinc nitrate, 1.5 mL DEF, .5 mL ethanol, 1.0 M nitric acid (50 μL, .05 mmol) in ethanol
  • 2.) Sonification
  • 3.) Heat 24 hours, cool down 9 hours

03-19-13

  • 4.) Filtration

03-20-13

  • 5.) Powder X-Ray Diffraction (See Image 1 below)

Sheets