Difference between revisions of "User:Ellen Petersen/Notebook/MOF Continued/2013/03/06"

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(Remove amorphous material in PPF-18)
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03-06-13
 
03-06-13
  
* 4.)
+
*Synthesizing Sheets:
 +
*1.) Add 7.9 mg (0.01 mmol) TCPP, 8.9 (0.03 mmmol) zinc nitrate, 1.5 mL DEF, .5 mL ethanol, 1.0 M nitric acid (50 μL, .05 mmol) in ethanol
 +
*2.) Sonification
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*3.) Heat 24 hours, cool down 9 hours
 +
03-19-13
 +
 
 +
*4.) Filtration
 +
 
 +
03-20-13
 +
 
 +
*5.) Powder X-Ray Diffraction (See Image 1 below)
 +
 
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[[Image:032013.png‎|200px|Description of image]]
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03-08-13
 
03-08-13
  

Revision as of 05:16, 28 June 2013

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Remove amorphous material in PPF-18

  • 1.) Combine Vials ( EK 2/4/13, EMP 11/16/13, AEM 1/8/13, AEM 1/28/13)
  • 2.) Add .0092 g to small vial
  • 3.) Add 1.5 mL DEF, .5 mL ethanol, .0175014 g Adenine

_________________________________________________________________________________________________________________ 03-06-13

  • Synthesizing Sheets:
  • 1.) Add 7.9 mg (0.01 mmol) TCPP, 8.9 (0.03 mmmol) zinc nitrate, 1.5 mL DEF, .5 mL ethanol, 1.0 M nitric acid (50 μL, .05 mmol) in ethanol
  • 2.) Sonification
  • 3.) Heat 24 hours, cool down 9 hours

03-19-13

  • 4.) Filtration

03-20-13

  • 5.) Powder X-Ray Diffraction (See Image 1 below)

Description of image

03-08-13

  • 4.)Filter