Difference between revisions of "User:Ellen Petersen/Notebook/MOF Continued/2013/03/06"

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|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> MOF: Tara </span>
 
|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> MOF: Tara </span>
|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}}
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|style="background-color: #F2F2F2" align="center"|[[File:Report.png|frameless|link={{#sub:{{FULLPAGENAME}}|0|-11}}]][[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|[[File:Resultset_previous.png|frameless|link={{#lnpreventry:{{FULLPAGENAME}}}}]][[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]][[File:Resultset_next.png|frameless|link={{#lnnextentry:{{FULLPAGENAME}}}}]]}}
 
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==Remove amorphous material in PPF-18==
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==Remove amorphous material in PPF-18 & Synthesizing Sheets==
 +
 
 
* 1.) Combine Vials ( EK 2/4/13, EMP 11/16/13, AEM 1/8/13, AEM 1/28/13)
 
* 1.) Combine Vials ( EK 2/4/13, EMP 11/16/13, AEM 1/8/13, AEM 1/28/13)
 
* 2.) Add .0092 g to small vial
 
* 2.) Add .0092 g to small vial
 
* 3.) Add 1.5 mL DEF, .5 mL ethanol, .0175014 g Adenine
 
* 3.) Add 1.5 mL DEF, .5 mL ethanol, .0175014 g Adenine
 +
 +
*Powder X-Ray Diffraction taken of PPF-18, and PPF-18 with adenine
 +
 +
 +
[[Image:31313.png‎|200px|PPF-18]]
 +
 +
[[Image:031313.png‎|200px|PPF-18 with Adenine]]
 +
 +
[[Image:032713.png‎|200px|PPF-18 with Adenine]]
 
_________________________________________________________________________________________________________________
 
_________________________________________________________________________________________________________________
 
03-06-13
 
03-06-13
  
* 4.)
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*Synthesizing Sheets:
03-08-13
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*1.) Add 7.9 mg (0.01 mmol) TCPP, 8.9 (0.03 mmmol) zinc nitrate, 1.5 mL DEF, .5 mL ethanol, 1.0 M nitric acid (50 μL, .05 mmol) in ethanol
 +
*2.) Sonification
 +
*3.) Heat 24 hours, cool down 9 hours
 +
03-19-13
 +
 
 +
*4.) Filtration
 +
 
 +
03-20-13
 +
 
 +
*5.) Powder X-Ray Diffraction (See Image 1 below)
 +
 
 +
[[Image:032012.png‎|200px|Sheets]]
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* 4.)Filter 
 
 
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__NOTOC__
 
__NOTOC__

Latest revision as of 22:52, 26 September 2017

Owwnotebook icon.png MOF: Tara Report.pngMain project page
Resultset previous.pngPrevious entry      Next entryResultset next.png

Remove amorphous material in PPF-18 & Synthesizing Sheets

  • 1.) Combine Vials ( EK 2/4/13, EMP 11/16/13, AEM 1/8/13, AEM 1/28/13)
  • 2.) Add .0092 g to small vial
  • 3.) Add 1.5 mL DEF, .5 mL ethanol, .0175014 g Adenine
  • Powder X-Ray Diffraction taken of PPF-18, and PPF-18 with adenine


PPF-18

PPF-18 with Adenine

PPF-18 with Adenine _________________________________________________________________________________________________________________ 03-06-13

  • Synthesizing Sheets:
  • 1.) Add 7.9 mg (0.01 mmol) TCPP, 8.9 (0.03 mmmol) zinc nitrate, 1.5 mL DEF, .5 mL ethanol, 1.0 M nitric acid (50 μL, .05 mmol) in ethanol
  • 2.) Sonification
  • 3.) Heat 24 hours, cool down 9 hours

03-19-13

  • 4.) Filtration

03-20-13

  • 5.) Powder X-Ray Diffraction (See Image 1 below)

Sheets