Difference between revisions of "User:Ellen Petersen/Notebook/MOF Continued/2013/03/04"

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(Filtering DPNI)
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* 3.)Rotavap to separate solvent and solute, leftover is dark brown liquid
 
* 3.)Rotavap to separate solvent and solute, leftover is dark brown liquid
 
* NMR: Liquid from Rotavap- Image 1
 
* NMR: Liquid from Rotavap- Image 1
* NMR: Solid from filtration- Figure 2
+
* NMR: Solid from filtration- Image 2
 +
 
 +
[[Image:030813-1.png‎|200px|NMR: Liquid from Rotavap]]
 +
[[Image:030813-1.png‎|200px|NMR: Solid from filtration]]
  
 
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Revision as of 06:08, 28 June 2013

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Filtering DPNI

  • 1.) Add 550 mL ethanol,
  • 2.) Vacuum Filtration to separate filter paper from DPNI solid

_____________________________________________________________________________________________________________________________ 03-05-2013

  • 3.)Rotavap to separate solvent and solute, leftover is dark brown liquid
  • NMR: Liquid from Rotavap- Image 1
  • NMR: Solid from filtration- Image 2

NMR: Liquid from Rotavap NMR: Solid from filtration