User:Ellen Petersen/Notebook/MOF Continued/2013/03/04

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Filtering DPNI

  • 1.) Add 550 mL ethanol,
  • 2.) Vacuum Filtration to separate filter paper from DPNI solid

_____________________________________________________________________________________________________________________________ 03-05-2013

  • 3.)Rotavap to separate solvent and solute, leftover is dark brown liquid
  • NMR: Liquid from Rotavap- Image 1
  • NMR: Solid from filtration- Figure 2