Difference between revisions of "User:Ellen Petersen/Notebook/MOF/2013/07/01"

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|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> MOF: Ellen</span>
 
|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> MOF: Ellen</span>
|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}}
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|style="background-color: #F2F2F2" align="center"|[[File:Report.png|frameless|link={{#sub:{{FULLPAGENAME}}|0|-11}}]][[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|[[File:Resultset_previous.png|frameless|link={{#lnpreventry:{{FULLPAGENAME}}}}]][[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]][[File:Resultset_next.png|frameless|link={{#lnnextentry:{{FULLPAGENAME}}}}]]}}
 
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*1.) Add .5 g Zinc nitrate hexahydrate,.209 g terephthalic acid, 5 mL DMF to a small capped vial
 
*1.) Add .5 g Zinc nitrate hexahydrate,.209 g terephthalic acid, 5 mL DMF to a small capped vial
 
*2.) Sonicated until clear
 
*2.) Sonicated until clear
*3.) Heated at 80 degree C
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*3.) Heated at 80 degree C and left overnight to heat
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_______________________________________________________________________________________________________________________________________________
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07-02-13
  
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*4.)Took out of oven (see image below)
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[[Image:070213.png‎|200px|MOF-5]]
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*5.) After cooling, vacuum filtration
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*6.) Run Powder X-Ray Diffraction (see Image below)
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[[Image:70213.png‎|200px|MOF-5]]
  
 
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Latest revision as of 21:54, 26 September 2017

Owwnotebook icon.png MOF: Ellen Report.pngMain project page
Resultset previous.pngPrevious entry      Next entryResultset next.png

MOF-5

  • 1.) Add .5 g Zinc nitrate hexahydrate,.209 g terephthalic acid, 5 mL DMF to a small capped vial
  • 2.) Sonicated until clear
  • 3.) Heated at 80 degree C and left overnight to heat

_______________________________________________________________________________________________________________________________________________ 07-02-13

  • 4.)Took out of oven (see image below)

MOF-5

  • 5.) After cooling, vacuum filtration
  • 6.) Run Powder X-Ray Diffraction (see Image below)


MOF-5