User:Ellen Petersen/Notebook/MOF/2013/07/01: Difference between revisions
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|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> MOF: Ellen</span> | |style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> MOF: Ellen</span> | ||
|style="background-color: #F2F2F2" align="center"| | |style="background-color: #F2F2F2" align="center"|[[File:Report.png|frameless|link={{#sub:{{FULLPAGENAME}}|0|-11}}]][[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|[[File:Resultset_previous.png|frameless|link={{#lnpreventry:{{FULLPAGENAME}}}}]][[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]] }}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]][[File:Resultset_next.png|frameless|link={{#lnnextentry:{{FULLPAGENAME}}}}]]}} | ||
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*1.) Add .5 g Zinc nitrate hexahydrate,.209 g terephthalic acid, 5 mL DMF to a small capped vial | *1.) Add .5 g Zinc nitrate hexahydrate,.209 g terephthalic acid, 5 mL DMF to a small capped vial | ||
*2.) Sonicated until clear | *2.) Sonicated until clear | ||
*3.) Heated at 80 degree C | *3.) Heated at 80 degree C and left overnight to heat | ||
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07-02-13 | |||
*4.)Took out of oven (see image below) | |||
[[Image:070213.png|200px|MOF-5]] | |||
*5.) After cooling, vacuum filtration | |||
*6.) Run Powder X-Ray Diffraction (see Image below) | |||
[[Image:70213.png|200px|MOF-5]] | |||
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Latest revision as of 22:54, 26 September 2017
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MOF-5
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