User:Ellen Petersen/Notebook/MOF/2013/06/26: Difference between revisions
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* 10.) Solution stable at 135 degrees at 35, mark red line on it to see difference in solution level. | * 10.) Solution stable at 135 degrees at 35, mark red line on it to see difference in solution level. | ||
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06-27-13 | |||
* 11.) Turn off nitrogen and water, Cool to Room Temperature | |||
* 12.) Not enough diethyl ether, took 400 mL of diethyl ether (instead of the required 600 mL) and poured 2/3's of DPNI solution into the 400 mL of diethyl ether. | |||
* 13.) Filter out | |||
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07-02-13 | |||
*14.) Ran 1/4 of the DPNI with 150 mL of ethanol through the rotavap | |||
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07-05-13 | |||
*15.) Ran the rest of the DPNI with 150 mL of ethanol through the rotavap | |||
Revision as of 12:59, 8 July 2013
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DPNI: 06-26-13
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