Difference between revisions of "User:Ellen Petersen/Notebook/MOF/2013/06/26"

From OpenWetWare
< User:Ellen Petersen‎ | Notebook‎ | MOF‎ | 2013‎ | 06
Jump to: navigation, search
(Autocreate 2013/06/26 Entry for User:Ellen_Petersen/Notebook/MOF)
 
Line 1: Line 1:
 
{|{{table}} width="800"
 
{|{{table}} width="800"
 
|-
 
|-
|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span>
+
|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> MOF</span>
 
|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}}
 
|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}}
 
|-
 
|-
 
| colspan="2"|
 
| colspan="2"|
 
<!-- ##### DO NOT edit above this line unless you know what you are doing. ##### -->
 
<!-- ##### DO NOT edit above this line unless you know what you are doing. ##### -->
==Entry title==
+
==DPNI: 06-26-13==
* Insert content here...
+
 
 +
* 1.) Add solids 1,4,5,8 Naphthalenetetracarboxylic dianhydride (.805 g, 3.00 mmol) and 4-aminopyridine (.847 g, 6.00 mmol)to round bottom flask (I added .8054 g of 1,4,5,8 Naphthalenetetracarboxylic dianhydride, and .8479 g of 4-aminopyridine)
 +
* 2.) Add 150 mL of solvent (DMA) ~keep under hood~
 +
* 3.) Add Stir Bar to solution
 +
* 4.) Put under spout and raise black knob until there is enough pressure to hold it in place
 +
* 5.) Begin to stir
 +
* 6.) If attached to condenser, turn on water very slightly
 +
* 7.) Turn on nitrogen: ensure bubbles are about 1 every 4 seconds. (Turn little end of nossle up)
 +
* 8.) Turn on heat to 50, switch down accordingly until it reaches 135 degrees consistently.  
 +
* 9.) If solution seems to be boiling adjust and turn down
 +
* 10.) Solution stable at 135 degrees at 35, mark red line on it to see difference in solution level.
 +
______________________________________________________________________________________________________
  
  

Revision as of 10:01, 26 June 2013

Owwnotebook icon.png MOF <html><img src="/images/9/94/Report.png" border="0" /></html> Main project page
<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>Previous entry<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>Next entry<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>

DPNI: 06-26-13

  • 1.) Add solids 1,4,5,8 Naphthalenetetracarboxylic dianhydride (.805 g, 3.00 mmol) and 4-aminopyridine (.847 g, 6.00 mmol)to round bottom flask (I added .8054 g of 1,4,5,8 Naphthalenetetracarboxylic dianhydride, and .8479 g of 4-aminopyridine)
  • 2.) Add 150 mL of solvent (DMA) ~keep under hood~
  • 3.) Add Stir Bar to solution
  • 4.) Put under spout and raise black knob until there is enough pressure to hold it in place
  • 5.) Begin to stir
  • 6.) If attached to condenser, turn on water very slightly
  • 7.) Turn on nitrogen: ensure bubbles are about 1 every 4 seconds. (Turn little end of nossle up)
  • 8.) Turn on heat to 50, switch down accordingly until it reaches 135 degrees consistently.
  • 9.) If solution seems to be boiling adjust and turn down
  • 10.) Solution stable at 135 degrees at 35, mark red line on it to see difference in solution level.

______________________________________________________________________________________________________