User:Ellen Petersen/Notebook/MOF/2012/04/12

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DPNI Take 1

  • 1.) 1,4,5,8 Naphthalenetetracarboxylic dianhydride (.805g, 3.00 mmol)
  • 2.) 4- aminopyridine (.847 g, 6.00 mmol)
  • 3.) Diethyl ether (600 mL
  • 4.) Dimethylacetamide (DMA) (150 mL)

Dissolve 1&2 in DMA stirred at 135 degrees C overnight cooled to room temperature and poured onto diethyl ether (600 mL)

precipitate filter and washed with diethyl ether dried under vacuum to yield