Difference between revisions of "User:Ellen Petersen/Notebook/MOF/2012/04/12"

From OpenWetWare
< User:Ellen Petersen‎ | Notebook‎ | MOF‎ | 2012‎ | 04
Jump to: navigation, search
Line 12: Line 12:
 
*4.) Dimethylacetamide (DMA) (150 mL)
 
*4.) Dimethylacetamide (DMA) (150 mL)
  
*Dissolve 1&2 in DMA stirred at 135 degrees C overnight.
+
*5.) Dissolve 1&2 in DMA stirred at 135 degrees C overnight.
*Cooled to room temperature and poured onto diethyl ether (600 mL).
+
*6.) Cooled to room temperature and poured onto diethyl ether (600 mL).
  
*Precipitate filter and washed with diethyl ether
+
*7.) Precipitate filter and washed with diethyl ether
*dried under vacuum to yield  
+
*8.) dried under vacuum to yield  
  
  

Revision as of 08:43, 28 June 2013

Owwnotebook icon.png MOF <html><img src="/images/9/94/Report.png" border="0" /></html> Main project page
Next entry<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>

DPNI: 04-12-12

  • 1.) 1,4,5,8 Naphthalenetetracarboxylic dianhydride (.805g, 3.00 mmol)
  • 2.) 4- aminopyridine (.847 g, 6.00 mmol)
  • 3.) Diethyl ether (600 mL
  • 4.) Dimethylacetamide (DMA) (150 mL)
  • 5.) Dissolve 1&2 in DMA stirred at 135 degrees C overnight.
  • 6.) Cooled to room temperature and poured onto diethyl ether (600 mL).
  • 7.) Precipitate filter and washed with diethyl ether
  • 8.) dried under vacuum to yield