User:Ellen Petersen/Notebook/MOF/2012/04/12: Difference between revisions
From OpenWetWare
No edit summary |
|||
| (2 intermediate revisions by the same user not shown) | |||
| Line 1: | Line 1: | ||
{|{{table}} width="800" | {|{{table}} width="800" | ||
|- | |- | ||
|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> | |style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> MOF</span> | ||
|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html> </html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}} | |style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html> </html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}} | ||
|- | |- | ||
| colspan="2"| | | colspan="2"| | ||
<!-- ##### DO NOT edit above this line unless you know what you are doing. ##### --> | <!-- ##### DO NOT edit above this line unless you know what you are doing. ##### --> | ||
==DPNI | ==DPNI: 04-12-12== | ||
* 1.) 1,4,5,8 Naphthalenetetracarboxylic dianhydride (.805g, 3.00 mmol) | * 1.) 1,4,5,8 Naphthalenetetracarboxylic dianhydride (.805g, 3.00 mmol) | ||
*2.) 4- aminopyridine (.847 g, 6.00 mmol) | *2.) 4- aminopyridine (.847 g, 6.00 mmol) | ||
| Line 12: | Line 12: | ||
*4.) Dimethylacetamide (DMA) (150 mL) | *4.) Dimethylacetamide (DMA) (150 mL) | ||
*Dissolve 1&2 in DMA stirred at 135 degrees C overnight. | *5.) Dissolve 1&2 in DMA stirred at 135 degrees C overnight. | ||
*Cooled to room temperature and poured onto diethyl ether (600 mL). | *6.) Cooled to room temperature and poured onto diethyl ether (600 mL). | ||
*Precipitate filter and washed with diethyl ether | *7.) Precipitate filter and washed with diethyl ether | ||
*dried under vacuum to yield | *8.) dried under vacuum to yield | ||
Revision as of 08:43, 28 June 2013
 MOF
|
<html><img src="/images/9/94/Report.png" border="0" /></html> Main project page Next entry<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html> |
DPNI: 04-12-12
| |
