Difference between revisions of "User:Ellen Petersen/Notebook/MOF/2012/04/12"

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|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span>
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|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}}
 
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==DPNI Take 1==
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==DPNI: 04-12-12==
 
* 1.) 1,4,5,8 Naphthalenetetracarboxylic dianhydride (.805g, 3.00 mmol)
 
* 1.) 1,4,5,8 Naphthalenetetracarboxylic dianhydride (.805g, 3.00 mmol)
 
*2.) 4- aminopyridine (.847 g, 6.00 mmol)
 
*2.) 4- aminopyridine (.847 g, 6.00 mmol)
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*4.) Dimethylacetamide (DMA) (150 mL)
 
*4.) Dimethylacetamide (DMA) (150 mL)
  
*Dissolve 1&2 in DMA stirred at 135 degrees C overnight.
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*5.) Dissolve 1&2 in DMA stirred at 135 degrees C overnight.
*Cooled to room temperature and poured onto diethyl ether (600 mL).
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*6.) Cooled to room temperature and poured onto diethyl ether (600 mL).
  
*Precipitate filter and washed with diethyl ether
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*7.) Precipitate filter and washed with diethyl ether
*dried under vacuum to yield  
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*8.) dried under vacuum to yield  
  
  

Revision as of 07:43, 28 June 2013

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DPNI: 04-12-12

  • 1.) 1,4,5,8 Naphthalenetetracarboxylic dianhydride (.805g, 3.00 mmol)
  • 2.) 4- aminopyridine (.847 g, 6.00 mmol)
  • 3.) Diethyl ether (600 mL
  • 4.) Dimethylacetamide (DMA) (150 mL)
  • 5.) Dissolve 1&2 in DMA stirred at 135 degrees C overnight.
  • 6.) Cooled to room temperature and poured onto diethyl ether (600 mL).
  • 7.) Precipitate filter and washed with diethyl ether
  • 8.) dried under vacuum to yield