Difference between revisions of "User:Ellen Petersen/Notebook/MOF/2012/04/12"

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(Entry title)
(DPNI Take 1)
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*4.) Dimethylacetamide (DMA) (150 mL)
 
*4.) Dimethylacetamide (DMA) (150 mL)
  
Dissolve 1&2 in DMA stirred at 135 degrees C overnight
+
*Dissolve 1&2 in DMA stirred at 135 degrees C overnight.
cooled to room temperature and poured onto diethyl ether (600 mL)
+
*Cooled to room temperature and poured onto diethyl ether (600 mL).
  
precipitate filter and washed with diethyl ether
+
*Precipitate filter and washed with diethyl ether
dried under vacuum to yield  
+
*dried under vacuum to yield  
  
  

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DPNI Take 1

  • 1.) 1,4,5,8 Naphthalenetetracarboxylic dianhydride (.805g, 3.00 mmol)
  • 2.) 4- aminopyridine (.847 g, 6.00 mmol)
  • 3.) Diethyl ether (600 mL
  • 4.) Dimethylacetamide (DMA) (150 mL)
  • Dissolve 1&2 in DMA stirred at 135 degrees C overnight.
  • Cooled to room temperature and poured onto diethyl ether (600 mL).
  • Precipitate filter and washed with diethyl ether
  • dried under vacuum to yield