Difference between revisions of "User:Dhea Patel/Notebook/Phosphorylation/2012/10/03"

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(Description)
(Description)
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--150mL acetonitrile + saturated sodium nitrate
 
--150mL acetonitrile + saturated sodium nitrate
 +
 
--100mL 90% acetonitrile + saturated sodium nitrate
 
--100mL 90% acetonitrile + saturated sodium nitrate
 +
 
--150mL 80% acetonitrile + saturated sodium nitrate
 
--150mL 80% acetonitrile + saturated sodium nitrate
 +
 
--400mL 70% acetonitrile + saturated sodium nitrate
 
--400mL 70% acetonitrile + saturated sodium nitrate
 +
 
--200mL 65% acetonitrile + saturated sodium nitrate
 
--200mL 65% acetonitrile + saturated sodium nitrate
 +
  
 
2 bands appeared. The second one was collected and rotovapped.
 
2 bands appeared. The second one was collected and rotovapped.

Revision as of 07:55, 3 October 2012

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Objective

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Description

  1. 0.22g Ru complex was purified in a silcia gel column, using a total of about 1.5L acetonitrile.

--150mL acetonitrile + saturated sodium nitrate

--100mL 90% acetonitrile + saturated sodium nitrate

--150mL 80% acetonitrile + saturated sodium nitrate

--400mL 70% acetonitrile + saturated sodium nitrate

--200mL 65% acetonitrile + saturated sodium nitrate


2 bands appeared. The second one was collected and rotovapped.

Data

  • Add data and results here...

Notes

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