Difference between revisions of "User:Allison K. Alix/Notebook/CHEM-581/2012/09/14"

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==Description==
 
==Description==
 
   
 
   
0.1g of polyvinyl alochol film (0.5 g in 6mL H2O) treated with gluteraldehyde was placed in a solution containing 100mL water, 2mL HCl, and 20g Na2SO4 @ 70 degrees celsius. The sodium sulfate is added to decrease solubility of the polymer during the acetalization reaction. The polymer film was immersed in solution with stirring for 1 hour. A 1% HCl solution was prepared and heated to 70 degrees celsius.
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0.1g of polyvinyl alochol film (0.5 g in 6mL H2O) treated with gluteraldehyde was placed in a solution containing 100mL water, 2mL HCl, and 20g Na2SO4 @ 70 degrees celsius. The sodium sulfate is added to decrease solubility of the polymer during the acetalization reaction. The polymer film was immersed in solution with stirring for 1 hour. The film was then rinsed with water and immersed in a 1% HCl solution @ 70 degrees celsius for 1/2 hour.
  
 
==Data==
 
==Data==

Revision as of 10:39, 14 September 2012

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Objective

In Situ cross-linking of polyvinyl alcohol films

Description

0.1g of polyvinyl alochol film (0.5 g in 6mL H2O) treated with gluteraldehyde was placed in a solution containing 100mL water, 2mL HCl, and 20g Na2SO4 @ 70 degrees celsius. The sodium sulfate is added to decrease solubility of the polymer during the acetalization reaction. The polymer film was immersed in solution with stirring for 1 hour. The film was then rinsed with water and immersed in a 1% HCl solution @ 70 degrees celsius for 1/2 hour.

Data

  • Add data and results here...

Notes

See NASA Technical Paper 1407