Difference between revisions of "User:Abigail E. Miller/Notebook/MOF Project/2013/02/04"

From OpenWetWare
Jump to: navigation, search
(Autocreate 2013/02/04 Entry for User:Abigail_E._Miller/Notebook/MOF_Project)
 
Line 7: Line 7:
 
<!-- ##### DO NOT edit above this line unless you know what you are doing. ##### -->
 
<!-- ##### DO NOT edit above this line unless you know what you are doing. ##### -->
 
==Objective==
 
==Objective==
* Insert content here...
+
* finish sampels from Jan 31st, 2013
  
 
==Bench Work==
 
==Bench Work==
* Insert content here...
+
* filtered the product from the DO2A reacting with zinc nitrate.  
 +
** collected brown crystals
 +
** collected a powder XRD pattern
 +
 
 +
* collected a powder XRD pattern for PPF-27 from 1/31/2013
 +
 
 +
* filtered and washed the PPF-18 from Eleni's three reaction vials repared on 1/31/2013
 +
** collected 30 mg of purple crystals.
 +
** collected a powder XRD pattern
  
 
==Data/Spectra==
 
==Data/Spectra==
Line 16: Line 24:
  
 
==Notes==
 
==Notes==
* Insert content here...
+
* low signal on all pXRDs. no peaks about 200 cnts. low intensity peaks lost in the noise.
  
 
<!-- ##### DO NOT edit below this line unless you know what you are doing. ##### -->
 
<!-- ##### DO NOT edit below this line unless you know what you are doing. ##### -->

Revision as of 14:54, 5 February 2013

Owwnotebook icon.png Metal Organic Frameworks <html><img src="/images/9/94/Report.png" border="0" /></html> Main project page
<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>Previous entry<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>Next entry<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>

Objective

  • finish sampels from Jan 31st, 2013

Bench Work

  • filtered the product from the DO2A reacting with zinc nitrate.
    • collected brown crystals
    • collected a powder XRD pattern
  • collected a powder XRD pattern for PPF-27 from 1/31/2013
  • filtered and washed the PPF-18 from Eleni's three reaction vials repared on 1/31/2013
    • collected 30 mg of purple crystals.
    • collected a powder XRD pattern

Data/Spectra

  • Insert content here...

Notes

  • low signal on all pXRDs. no peaks about 200 cnts. low intensity peaks lost in the noise.