User:Abigail E. Miller/Notebook/MOF Project/2013/01/23: Difference between revisions
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==Bench Work== | ==Bench Work== | ||
* | * 9am removed DO2A plus zinc reaction from the solution | ||
** yellowish solution with white suspension | |||
** white solid material on bottom and sides of vial | |||
** let cool to room temp on the bench t | |||
* also removed PPF18 and PPF18A samples from powder XRD | |||
** sensor, went off due to over heating of the X ray source | |||
* exchanging DPNI for adenine | |||
** mixed 0.5 mL of ethanol and 1.5 mL DEF | |||
** added 0.0070 mg adenine, but it did not all dissolve | |||
** collected UVVis spectrum of solution | |||
*Weight of PPF18 | |||
** paper 0.1332 g | |||
**paper plus PPF18 0.1528 g | |||
** after putting in 10mL beaker, paper 0.1332 g | |||
**Some loss of material to static | |||
* 10:20am added 1mL of adenine solution to PPF18 | |||
** waiting 3 hrs | |||
* filtered material from DO2A and zinc reaction | |||
* 1:30 pm filtered PPF18 with adenine | |||
** filtrate was purple - indicates presence of porphyrin, dissolved from the PPf18 | |||
** washed with DEF | |||
==Data/Spectra== | ==Data/Spectra== | ||
Revision as of 10:42, 25 January 2013
 Metal Organic Frameworks
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Objective
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