User:Moira M. Esson/Notebook/CHEM-581/2013/04/05: Difference between revisions
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#Repeat 1-3 twice. | #Repeat 1-3 twice. | ||
# The samples remained in the fume hood over night without a cap to ensure complete removal of all hexanes. | # The samples remained in the fume hood over night without a cap to ensure complete removal of all hexanes. | ||
<br> | |||
==Pressure Testing== | |||
*Pressure testing using an unmodified pipette was completed. | |||
* The general protocol for fluorescence was followed. | |||
* The specific parameters included: | |||
# Excitation Slit Width: 10 | |||
# Emission Slit Width: 10 | |||
# Scan Speed: 1200 | |||
*The general protocol for unmodified pressure testing described on [[ | |||
Table 1. Samples that were used for unmodified pressure testing | |||
<br> | |||
{| {{table}} | |||
| align="center" style="background:#f0f0f0;"|'''Sample Order''' | |||
| align="center" style="background:#f0f0f0;"|'''PVOH vs. Clay Ratio''' | |||
| align="center" style="background:#f0f0f0;"|'''PVOH Type''' | |||
| align="center" style="background:#f0f0f0;"|'''Clay Selection''' | |||
| align="center" style="background:#f0f0f0;"|'''Amount of Hydrogel Used (g)''' | |||
|- | |||
| 1||50:50||146K||110% CEC Laponite w/ DMHXLBR||0.1883 | |||
|- | |||
| 2||90:10||146K||NaMT||0.1742 | |||
|- | |||
| 3||90:10||146K||110% CEC Laponite w/ DMHXLBR||0.1404 | |||
|- | |||
| 4||90:10||146K||50% CEC NaMT w/ Bu<sub>3</sub>HdP<sup>+</sup>||0.1721 | |||
|- | |||
| 5||50:50||146K||50% CEC NaMT w/ Bu<sub>3</sub>HdP<sup>+</sup>||0.1884 | |||
|- | |||
| 6||50:50||146K||NaMT||0.1349 | |||
|} | |||
<br> | <br> | ||
Revision as of 07:07, 15 April 2013
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Objectives
Microsphere Work-UpDecanting: The general protocol described on 2013/03/01 was followed.
Pressure Testing
# Excitation Slit Width: 10 # Emission Slit Width: 10 # Scan Speed: 1200
Table 1. Samples that were used for unmodified pressure testing
Notes
|