Synthesis of new films was started. The procedure may be viewed here.
Finish the synthesis of clay films started on 09/03. The procedure may be viewed here.
Fourier Transform Infrared Spectroscopy (FTIR)
We will be using attenuated total reflectance (ATR) mode for our samples
Place the film in the sample holder. Execute measurement
Save measurement data onto thumb drive
DSC
Weigh the pan and lid with no sample
cut a piece of sample with a razor blade that is ≤3mg
Seal the lid on the pan
Place pans into the DSC and set up the instrument
Wait for all measurements to be taken
New Film Data
Film Synthesis
0.9997g PVA
1.0142g PVA +0.1038g Cloisite
DSC Prep Data
==FTIR of MG Sample Film Data
Notes
When handling the pans in preparation for the DSC, two different sets of forceps should be used. One for handling the films and one for handling the pan. The reason being that water on the outside of the pan will skew measurements.
This is a visual of the different films and their absorbance of the Malachite Green.