User:Elaine Marie Robbins/Notebook/MOF/2012/06/04

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Powder XRD for PPF-18 Main project page
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Methods

  1. Run powder XRD on PPF-18 synthesized by Dr. Miller on 05/14/12.
  2. Synthesize PPF-27 from PPF-18.
    1. Combine 2.0 mg of PPF-18, 3.2 mg BPY, 1.5 mL DEF, and 0.5 mL EtOH.
    2. Swirl and allow to react for 3 hr.

Data

  • XRD data of PPF-18:

Scan speed: 0.2 deg/min.

Sampling width: 0.010 degrees.


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