User:Tamanika Tinsley/Notebook/Chem 581 Biomaterials Design Lab/2014/09/26: Difference between revisions

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|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span>
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|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}}
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==Objective==
==Objective==
*Create duplicate films from the ion exchanged clays
*Create duplicate films from the ion exchanged clays
'''[http://openwetware.org/wiki/User:Tamanika_Tinsley/Notebook/Chem_581_Biomaterials_Design_Lab/2014/09/24 The films were created using the procedure from 9/24]
'''[http://openwetware.org/wiki/User:Tamanika_Tinsley/Notebook/Chem_581_Biomaterials_Design_Lab/2014/09/24 The films were created using the procedure from 9/24]'''


'''*Finish processing the clays from 9/24/2014
*Finish processing the clays from 9/24/2014


'''Completing film synthesis'''  
'''Completing film synthesis'''  
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*Place film in 1% HCl Solution (see below for details) at 80C for 30 minutes with gentle stirring  
*Place film in 1% HCl Solution (see below for details) at 80C for 30 minutes with gentle stirring  
* Place film in Sodium Bicarbonate Solution for 15 minutes at room temperature with gentle stirring  
* Place film in Sodium Bicarbonate Solution for 15 minutes at room temperature with gentle stirring  
==Ion Exchanged Films==
#The PVA with (1-hexadecyl) triphenylphosphonium bromide film from Eleni's group looked homogeneous, with a light brown color.
#Below is a picture of the PVA with tributylhexadecylphosphonium bromide made by my group. In this case the clay was not evenly dispersed.
[[Image:IMG 3795.JPG|800x580px|center|thumb]]




Latest revision as of 00:21, 27 September 2017

Project name Main project page
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Sept 26 - Creation of ion exchanged films

  • Group Members Andrew Farag Sr (Undergrad) and Michael Bible Jr (Undergrad)
  • Group Name : AMT

Objective

  • Create duplicate films from the ion exchanged clays

The films were created using the procedure from 9/24

  • Finish processing the clays from 9/24/2014

Completing film synthesis

The ion exchanged clays were processed using the procedure from 8/29/2014

  • Warm 150mL of Sodium Sulfate Solution (see below for details) at 80C for 15 minutes
  • Place film in Sodium Sulfate Solution (see below for details) at 80C for 1 hour with gentle stirring
  • Warm 150mL of 1% HCl at 80C for 15 minutes
  • Place film in 1% HCl Solution (see below for details) at 80C for 30 minutes with gentle stirring
  • Place film in Sodium Bicarbonate Solution for 15 minutes at room temperature with gentle stirring

Ion Exchanged Films

  1. The PVA with (1-hexadecyl) triphenylphosphonium bromide film from Eleni's group looked homogeneous, with a light brown color.
  2. Below is a picture of the PVA with tributylhexadecylphosphonium bromide made by my group. In this case the clay was not evenly dispersed.



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