User:Samiye Yaman/Notebook/Lab 581/2013/01/30 - Revision history

Samiye Yaman: /* Description */

2013-02-06T16:01:14Z

Description

←Older revision		Revision as of 16:01, 6 February 2013
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	*prepare 2 sets of each		*prepare 2 sets of each

-	1)0.5g PVOH (MW:22,000) + 6 ml water ~~<b>[[User:Matt Hartings\|Matt Hartings]] 0.5g of what???</b>~~	+	1)0.5g PVOH (MW:22,000) + 6 ml water

	2)0.5 PVOH (MW:89,000-98,000) + 6 ml water		2)0.5 PVOH (MW:89,000-98,000) + 6 ml water
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	*0.5 g of PVOH was mixed with 6ml of water then was placed in to a hot plate with temperature of 90C. The solution was stirred and kept on the hot plate until PVOH was completely dissolved.Once it was completely dissolved, 6μ of R6G in to each beaker was added then they were placed in to a freezer (at -20C)for 24 hours.The freezing and thawing method was repeated. 3 cycles were used.		*0.5 g of PVOH was mixed with 6ml of water then was placed in to a hot plate with temperature of 90C. The solution was stirred and kept on the hot plate until PVOH was completely dissolved.Once it was completely dissolved, 6μ of R6G in to each beaker was added then they were placed in to a freezer (at -20C)for 24 hours.The freezing and thawing method was repeated. 3 cycles were used.
-
-	~~<b>[[User:Matt Hartings\|Matt Hartings]] there is a μL symbol you can use down below</b>~~
-
-
-	<b>[[User:Matt Hartings\|Matt Hartings]] You should also add a description of your full procedure for this process here. Why are you doing these things. At some point you'll have to mention it. This (the first page of your notebook) is the best place to do it.</b>

	==Data==		==Data==

Samiye Yaman: /* Description */

2013-02-06T15:19:10Z

Description

←Older revision		Revision as of 15:19, 6 February 2013
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	4)0.5g PVOH (MW:146,000-186,000) + 6ml of water		4)0.5g PVOH (MW:146,000-186,000) + 6ml of water

-	*0.5 g of PVOH was mixed with 6ml of water then was placed in to a hot plate with temperature of 90C. The solution was stirred and kept on the hot plate until PVOH was completely dissolved. The beaker was placed in to a freezer (at -20C)for 24 hours.	+	*0.5 g of PVOH was mixed with 6ml of water then was placed in to a hot plate with temperature of 90C. The solution was stirred and kept on the hot plate until PVOH was completely dissolved. The beaker was placed in to a freezer (at -20C)for 24 hours. After 24 hours, they removed from the freezer and stayed at room temperature for 24 hours. This is called freezing and thawing method. The cycle was repeated for 3 times.

	*placed into -20C at 10:10 for 1) and 2), 3), and 4) at 10:20.		*placed into -20C at 10:10 for 1) and 2), 3), and 4) at 10:20.
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-	*0.5 g of PVOH was mixed with 6ml of water then was placed in to a hot plate with temperature of 90C. The solution was stirred and kept on the hot plate until PVOH was completely dissolved.Once it was completely dissolved, 6μ of R6G in to each beaker was added then they were placed in to a freezer (at -20C)for 24 hours.	+	*0.5 g of PVOH was mixed with 6ml of water then was placed in to a hot plate with temperature of 90C. The solution was stirred and kept on the hot plate until PVOH was completely dissolved.Once it was completely dissolved, 6μ of R6G in to each beaker was added then they were placed in to a freezer (at -20C)for 24 hours.The freezing and thawing method was repeated. 3 cycles were used.

	<b>[[User:Matt Hartings\|Matt Hartings]] there is a μL symbol you can use down below</b>		<b>[[User:Matt Hartings\|Matt Hartings]] there is a μL symbol you can use down below</b>

Samiye Yaman: /* Description */

2013-02-06T15:15:51Z

Description

←Older revision		Revision as of 15:15, 6 February 2013
Line 18:		Line 18:
	*prepare 2 sets of each		*prepare 2 sets of each

-	1)0.5g of 22,000 + 6 ml water <b>[[User:Matt Hartings\|Matt Hartings]] 0.5g of what???</b>	+	1)0.5g PVOH (MW:22,000) + 6 ml water <b>[[User:Matt Hartings\|Matt Hartings]] 0.5g of what???</b>

-	2)0.5 of 89,000-98,000 + 6 ml water	+	2)0.5 PVOH (MW:89,000-98,000) + 6 ml water

-	3)0.5g of 130,000 + 6 ml of water	+	3)0.5g PVOH (MW:130,000) + 6 ml of water

-	4)0.5g of 146,000-186,000 + 6ml of water	+	4)0.5g PVOH (MW:146,000-186,000) + 6ml of water
		+
		+	*0.5 g of PVOH was mixed with 6ml of water then was placed in to a hot plate with temperature of 90C. The solution was stirred and kept on the hot plate until PVOH was completely dissolved. The beaker was placed in to a freezer (at -20C)for 24 hours.

	*placed into -20C at 10:10 for 1) and 2), 3), and 4) at 10:20.		*placed into -20C at 10:10 for 1) and 2), 3), and 4) at 10:20.
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	4)0.5g of 146,000-186,000 + 6ml of water		4)0.5g of 146,000-186,000 + 6ml of water

-	*add 6micL of R6G in to each hydrogels. <b>[[User:Matt Hartings\|Matt Hartings]] there is a μL symbol you can use down below</b>

-	*placed ~~into~~ -20C ~~at noon~~.	+	*0.5 g of PVOH was mixed with 6ml of water then was placed in to a hot plate with temperature of 90C. The solution was stirred and kept on the hot plate until PVOH was completely dissolved.Once it was completely dissolved, 6μ of R6G in to each beaker was added then they were placed in to a freezer (at -20C)for 24 hours.
		+
		+	<b>[[User:Matt Hartings\|Matt Hartings]] there is a μL symbol you can use down below</b>
		+

	<b>[[User:Matt Hartings\|Matt Hartings]] You should also add a description of your full procedure for this process here. Why are you doing these things. At some point you'll have to mention it. This (the first page of your notebook) is the best place to do it.</b>		<b>[[User:Matt Hartings\|Matt Hartings]] You should also add a description of your full procedure for this process here. Why are you doing these things. At some point you'll have to mention it. This (the first page of your notebook) is the best place to do it.</b>

Matt Hartings: /* Description */

2013-02-06T01:19:32Z

Description

←Older revision		Revision as of 01:19, 6 February 2013
Line 18:		Line 18:
	*prepare 2 sets of each		*prepare 2 sets of each

-	1)0.5g of 22,000 + 6 ml water	+	1)0.5g of 22,000 + 6 ml water <b>[[User:Matt Hartings\|Matt Hartings]] 0.5g of what???</b>

	2)0.5 of 89,000-98,000 + 6 ml water		2)0.5 of 89,000-98,000 + 6 ml water
Line 42:		Line 42:
	4)0.5g of 146,000-186,000 + 6ml of water		4)0.5g of 146,000-186,000 + 6ml of water

-	*add 6micL of R6G in to each hydrogels.	+	*add 6micL of R6G in to each hydrogels. <b>[[User:Matt Hartings\|Matt Hartings]] there is a μL symbol you can use down below</b>

	*placed into -20C at noon.		*placed into -20C at noon.
		+
		+	<b>[[User:Matt Hartings\|Matt Hartings]] You should also add a description of your full procedure for this process here. Why are you doing these things. At some point you'll have to mention it. This (the first page of your notebook) is the best place to do it.</b>

	==Data==		==Data==

Samiye Yaman: /* Data */

2013-02-01T19:37:04Z

Data

←Older revision		Revision as of 19:37, 1 February 2013
Line 47:		Line 47:

	==Data==		==Data==
-
-	*Film 1 dissolved during the filtration.
-
-	~~'''DSE Results'''~~

	==Notes==		==Notes==

Samiye Yaman: /* Description */

2013-01-30T16:45:55Z

Description

←Older revision		Revision as of 16:45, 30 January 2013
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	==Description==		==Description==

-	'''Part 1: ~~Filtration with different kinds of film~~'''	+	'''Part 1: Prepare hydrogels'''

-	*~~Film 1: 0.5g PVOH, gluteraldehyde (1ml)~~	+	*prepare 2 sets of each

-	*Film 2: NaMT PVOH	+	1)0.5g of 22,000 + 6 ml water

-	*Use 20 ml of CuSO4 during each filtration.	+	2)0.5 of 89,000-98,000 + 6 ml water

-	*Filtration done with 3 ~~different timings~~. ~~10 minutes~~, ~~30 minutes and 1 hour.~~	+	3)0.5g of 130,000 + 6 ml of water

		+	4)0.5g of 146,000-186,000 + 6ml of water

-	~~'''Part~~ 2~~'''~~	+	*placed into -20C at 10:10 for 1) and 2), 3), and 4) at 10:20.

-	*DSE measurement for	+	'''Part 2: Prepare Hydrogels with 0.5mM of R6G dye'''

-	1) 0.~~5g PVOH, gluteraldehyde~~ (~~1ml~~)	+	*0.00479 g of R6G dissolved in 10 ml of ethanol.(1mM)

-	~~2) 0~~.~~5 g PVOH (100000)+HCl+ Succinate acid~~	+	*take 10 micL and 9.99ml ethanol to make 1micM R6G.

-	3) 0.~~5 g PVOH (22000)~~+ 3 ml water ~~+ Mallic acid + phosphoric acid~~	+	1)0.5g of 22,000 + 6 ml water

-	4) ~~1 g PVOH (22000~~) + ~~phosphoric acid~~ + ~~Mallic acid~~	+	2)0.5 of 89,000-98,000 + 6 ml water
		+
		+	3)0.5g of 130,000 + 6 ml of water
		+
		+	4)0.5g of 146,000-186,000 + 6ml of water
		+
		+	*add 6micL of R6G in to each hydrogels.
		+
		+	*placed into -20C at noon.

	==Data==		==Data==

Samiye Yaman at 16:05, 30 January 2013

2013-01-30T16:05:37Z

←Older revision		Revision as of 16:05, 30 January 2013
Line 10:		Line 10:


		+	==Objective==

	==Description==		==Description==
-
-	*The course is designed by American University to experiment different aspects of PVOH films.

-	*During the course PVOH films with different ~~molecular weight will be produced. Effects~~ of ~~cross-linking, addition of different molecules such as gluteraldehyde, different acids, porphrin will be also tested.~~	+	'''Part 1: Filtration with different kinds of film'''

-	*~~UV-Vis spectrum~~, ~~Atomic Absorption spectrum~~, ~~X-Ray, FTIR, DMA, ISE~~ and ~~many other instruments will~~ be used to ~~analyze~~ the ~~results~~.	+	*Film 1: 0.5g PVOH, gluteraldehyde (1ml)
		+
		+	*Film 2: NaMT PVOH
		+
		+	*Use 20 ml of CuSO4 during each filtration.
		+
		+	*Filtration done with 3 different timings. 10 minutes, 30 minutes and 1 hour.
		+
		+
		+	'''Part 2'''
		+
		+	*DSE measurement for
		+
		+	1) 0.5g PVOH, gluteraldehyde (1ml)
		+
		+	2) 0.5 g PVOH (100000)+HCl+ Succinate acid
		+
		+	3) 0.5 g PVOH (22000)+ 3 ml water + Mallic acid + phosphoric acid
		+
		+	4) 1 g PVOH (22000) + phosphoric acid + Mallic acid
		+
		+	==Data==
		+
		+	*Film 1 dissolved during the filtration.
		+
		+	'''DSE Results'''
		+
		+	==Notes==
		+	This area is for any observations or conclusions that you would like to note.
		+
		+
		+	Use categories like tags. Change the "Course" category to the one corresponding to your course. The "Miscellaneous" tag can be used for particular experiments, as instructed by your professor. Please be sure to change or delete this tag as required so that the categories remain well organized.
		+
		+	[[Category:Course]]
		+	[[Category:Miscellaneous]]
		+
		+
		+
		+	<!-- ##### DO NOT edit below this line unless you know what you are doing. ##### -->
		+	\|}
		+
		+	__NOTOC__

Samiye Yaman: Autocreate 2013/01/30 Entry for User:Samiye_Yaman/Notebook/Lab_581

2013-01-30T13:45:27Z

Autocreate 2013/01/30 Entry for User:Samiye_Yaman/Notebook/Lab_581

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{|{{table}} width="800"
|-
|style="background-color: #EEE"|[[Image:BDLlogo_notext_lr.png|128px]]<span style="font-size:22px;"> Experimental Chemistry</span>
|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html>      </html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}}
|-
| colspan="2"|


==Description==

*The course is designed by American University to experiment different aspects of PVOH films.

*During the course PVOH films with different molecular weight will be produced. Effects of cross-linking, addition of different molecules such as gluteraldehyde, different acids, porphrin will be also tested.

*UV-Vis spectrum, Atomic Absorption spectrum, X-Ray, FTIR, DMA, ISE and many other instruments will be used to analyze the results.