User:Samiye Yaman/Notebook/Lab 581/2012/11/16 - Revision history

Samiye Yaman: /* Description */

Samiye Yaman — Fri, 16 Nov 2012 19:15:50 GMT

Description

←Older revision		Revision as of 19:15, 16 November 2012
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	*7 ml of HPLC film		*7 ml of HPLC film

-	*1 ml of porphyrin	+	*1 ml of porphyrin (conc: 97.42micM)

	*1 ml of gluteraldehyde		*1 ml of gluteraldehyde
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	''' Part 3: AA of the filtrates from 9/11/2012 & 14/11/2012'''		''' Part 3: AA of the filtrates from 9/11/2012 & 14/11/2012'''
		+
		+	*The filtrates had to be diluted.
		+
		+	*1 ml of each filtrate was mixed with 10 ml of HPLC water.
		+
		+	*Calculation(13 ppm of Cu ion was in the stick solution)
		+
		+	M(1)V(1)= M(2)*V(2)
		+
		+	13ppm1ml=M(2) *11ml
		+
		+	*M(2)=1.2 ppm

	==Data==		==Data==

Samiye Yaman: /* Data */

Samiye Yaman — Fri, 16 Nov 2012 19:11:27 GMT

Data

←Older revision		Revision as of 19:11, 16 November 2012
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	'''AA results'''		'''AA results'''
-
-	~~[[Image:Film_adsorption.png\|1000px]]~~
-

	*Actual concentration measured by AA of each filtrates are very close to each other except the number 2(gluteraldhyde filtrate of 30 min). (we stop the measurement too early therefore actual concentration of this filtrate should be ignored)		*Actual concentration measured by AA of each filtrates are very close to each other except the number 2(gluteraldhyde filtrate of 30 min). (we stop the measurement too early therefore actual concentration of this filtrate should be ignored)

	*AA results supports the UV-vis results from 14/11/1012.		*AA results supports the UV-vis results from 14/11/1012.
		+
		+	[[Image:Film_adsorption.png\|1000px]]

	==Notes==		==Notes==

Samiye Yaman: /* Data */

Samiye Yaman — Fri, 16 Nov 2012 19:11:03 GMT

Data

←Older revision		Revision as of 19:11, 16 November 2012
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	[[Image:Film_adsorption.png\|1000px]]		[[Image:Film_adsorption.png\|1000px]]
		+
		+
		+	*Actual concentration measured by AA of each filtrates are very close to each other except the number 2(gluteraldhyde filtrate of 30 min). (we stop the measurement too early therefore actual concentration of this filtrate should be ignored)
		+
		+	*AA results supports the UV-vis results from 14/11/1012.

	==Notes==		==Notes==

Samiye Yaman: /* Data */

Samiye Yaman — Fri, 16 Nov 2012 19:08:24 GMT

Data

←Older revision		Revision as of 19:08, 16 November 2012
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	==Data==		==Data==
		+
		+	'''AA results'''
		+
		+	[[Image:Film_adsorption.png\|1000px]]

	==Notes==		==Notes==

Samiye Yaman: /* Description */

Samiye Yaman — Fri, 16 Nov 2012 19:05:47 GMT

Description

←Older revision		Revision as of 19:05, 16 November 2012
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	*2 drops of HCl		*2 drops of HCl

-	'''AA of the filtrates from 9/11/2012 & 14/11/2012'''	+	''' Part 3: AA of the filtrates from 9/11/2012 & 14/11/2012'''

	==Data==		==Data==

Samiye Yaman: /* Description */

Samiye Yaman — Fri, 16 Nov 2012 19:05:28 GMT

Description

←Older revision		Revision as of 19:05, 16 November 2012
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	==Description==		==Description==

-	'''Part 1: ~~Filtration with different kinds~~ of ~~film~~'''	+	'''Part 1: Crosslinking of 2 of the films prepared on 14/11/2012'''

-	*Film 1: ~~0.5g PVOH, gluteraldehyde (1ml) cross-linked~~	+	'''Part 2: Prepare a film'''

-	*~~Film 2: 100%CEC NAMT~~	+	*0.5 g PVOH 2200

-	*~~Use 20~~ ml of ~~CuSO4 during each filtration.~~	+	*7 ml of HPLC film

-	*~~Filtration done with 3 different timings. 10 minutes, 30 minutes and~~ 1 ~~hour.~~	+	*1 ml of porphyrin
		+
		+	*1 ml of gluteraldehyde
		+
		+	*2 drops of HCl
		+
		+	'''AA of the filtrates from 9/11/2012 & 14/11/2012'''

	==Data==		==Data==

Samiye Yaman at 19:02, 16 November 2012

Samiye Yaman — Fri, 16 Nov 2012 19:02:24 GMT

←Older revision		Revision as of 19:02, 16 November 2012
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		+	==Objective==

	==Description==		==Description==
-
-	*The course is designed by American University to experiment different aspects of PVOH films.

-	*During the course PVOH films with different ~~molecular weight will be produced. Effects~~ of ~~cross-linking, addition of different molecules such as gluteraldehyde, different acids, porphrin will be also tested.~~	+	'''Part 1: Filtration with different kinds of film'''

-	*~~UV-Vis spectrum~~, ~~Atomic Absorption spectrum, X~~-~~Ray~~, ~~FTIR, DMA, ISE~~ and ~~many other instruments will~~ be used to ~~analyze~~ the ~~results~~.	+	*Film 1: 0.5g PVOH, gluteraldehyde (1ml) cross-linked
		+
		+	*Film 2: 100%CEC NAMT
		+
		+	*Use 20 ml of CuSO4 during each filtration.
		+
		+	*Filtration done with 3 different timings. 10 minutes, 30 minutes and 1 hour.
		+
		+	==Data==
		+
		+	==Notes==
		+	This area is for any observations or conclusions that you would like to note.
		+
		+
		+	Use categories like tags. Change the "Course" category to the one corresponding to your course. The "Miscellaneous" tag can be used for particular experiments, as instructed by your professor. Please be sure to change or delete this tag as required so that the categories remain well organized.
		+
		+	[[Category:Course]]
		+	[[Category:Miscellaneous]]
		+
		+
		+
		+	<!-- ##### DO NOT edit below this line unless you know what you are doing. ##### -->
		+	\|}
		+
		+	__NOTOC__

Samiye Yaman: Autocreate 2012/11/16 Entry for User:Samiye_Yaman/Notebook/Lab_581

Samiye Yaman — Fri, 16 Nov 2012 19:01:46 GMT

Autocreate 2012/11/16 Entry for User:Samiye_Yaman/Notebook/Lab_581

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{|{{table}} width="800"
|-
|style="background-color: #EEE"|[[Image:BDLlogo_notext_lr.png|128px]]<span style="font-size:22px;"> Experimental Chemistry</span>
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==Description==

*The course is designed by American University to experiment different aspects of PVOH films.

*During the course PVOH films with different molecular weight will be produced. Effects of cross-linking, addition of different molecules such as gluteraldehyde, different acids, porphrin will be also tested.

*UV-Vis spectrum, Atomic Absorption spectrum, X-Ray, FTIR, DMA, ISE and many other instruments will be used to analyze the results.