User:Samiye Yaman/Notebook/Lab 581/2012/11/02: Difference between revisions
From OpenWetWare
Samiye Yaman (talk | contribs) (Autocreate 2012/11/02 Entry for User:Samiye_Yaman/Notebook/Lab_581) |
(fix raw html notebook nav) |
||
(13 intermediate revisions by one other user not shown) | |||
Line 2: | Line 2: | ||
|- | |- | ||
|style="background-color: #EEE"|[[Image:BDLlogo_notext_lr.png|128px]]<span style="font-size:22px;"> Experimental Chemistry</span> | |style="background-color: #EEE"|[[Image:BDLlogo_notext_lr.png|128px]]<span style="font-size:22px;"> Experimental Chemistry</span> | ||
|style="background-color: #F2F2F2" align="center"| | |style="background-color: #F2F2F2" align="center"|[[File:Report.png|frameless|link={{#sub:{{FULLPAGENAME}}|0|-11}}]][[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|[[File:Resultset_previous.png|frameless|link={{#lnpreventry:{{FULLPAGENAME}}}}]][[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]] }}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]][[File:Resultset_next.png|frameless|link={{#lnnextentry:{{FULLPAGENAME}}}}]]}} | ||
|- | |- | ||
| colspan="2"| | | colspan="2"| | ||
Line 10: | Line 10: | ||
==Objective== | |||
==Description== | ==Description== | ||
* | '''Part 1 ''' | ||
*Place the porphyrin film (with 2 drops of HCL), prepared on 24/10/2012, into a 6 molality of NaCl with 100ml of HPLC water. | |||
*Place the NaCl solution in to a hot plate and wait until temperature raises to 70C. | |||
*At 70C place the film into beaker. | |||
'''Part 2''' | |||
*FTIR measurement for every film that has been prepared. | |||
==Data== | |||
'''Porphyrin film with 2 drops of HCL, prepared on 24/10/2012''' | |||
'''*Before cross-linking''' | |||
*The film shrunk and look more brittle. | |||
*More intense green color. | |||
[[Image:2012-10-31_11.23.11.jpg|500px]] | |||
'''*After cross-linking''' | |||
*The film expanded a little. | |||
*Less intense green color and looked more reddish brown. | |||
[[Image:2012-11-07_08.38.59.jpg|500px]] | |||
'''FTIR Results''' | |||
[[Image:1g22000PVOHcrosslinked.png|500px]] | |||
[[Image:1g22000PVOHH3PO4MaleicAcid.png|500px]] | |||
[[Image:1g22000PVOHH3PO4MaleicAcidcrosslinked.png|500px]] | |||
[[Image:1gPVOH22000H3PO4.png|500px]] | |||
[[Image:1gPVOH100000.png|500px]] | |||
[[Image:1gPVOH100000HCl.png|500px]] | |||
[[Image:1gPVOH100000HClcrosslinked.png|500px]] | |||
[[Image:Halfg22000PVOHgluteraldehyde.png|500px]] | |||
[[Image:Halfg100000PVOHcrosslinked.png|500px]] | |||
[[Image:HalfgPVOH2200.png|500px]] | |||
[[Image:HalfgPVOH22000H3PO4.png|500px]] | |||
[[Image:HalfgPVOH100000HCl.png|500px]] | |||
[[Image:HalfgPVOH100000HClSuccinicAcid.png|500px]] | |||
[[Image:OnetenthgPVOH22000.png|500px]] | |||
[[Image:OnetenthgPVOH100000.png|500px]] | |||
==Notes== | |||
This area is for any observations or conclusions that you would like to note. | |||
Use categories like tags. Change the "Course" category to the one corresponding to your course. The "Miscellaneous" tag can be used for particular experiments, as instructed by your professor. Please be sure to change or delete this tag as required so that the categories remain well organized. | |||
[[Category:Course]] | |||
[[Category:Miscellaneous]] | |||
<!-- ##### DO NOT edit below this line unless you know what you are doing. ##### --> | |||
|} | |||
__NOTOC__ |
Latest revision as of 22:11, 26 September 2017
Experimental Chemistry | Main project page Previous entry Next entry |
ObjectiveDescriptionPart 1
DataPorphyrin film with 2 drops of HCL, prepared on 24/10/2012 *Before cross-linking
*After cross-linking
FTIR Results NotesThis area is for any observations or conclusions that you would like to note.
|