User:Samiye Yaman/Notebook/Lab 581/2012/11/02

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'''Porphyrin film with 2 drops of HCL, prepared on 24/10/2012'''
'''Porphyrin film with 2 drops of HCL, prepared on 24/10/2012'''
-
*Before cross-linking
+
'''*Before cross-linking'''
*The film shrunk and look more brittle.
*The film shrunk and look more brittle.
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[[Image:2012-10-31_11.23.11.jpg|500px]]
[[Image:2012-10-31_11.23.11.jpg|500px]]
 +
 +
'''*After cross-linking'''
 +
 +
*The film expanded a little.
 +
 +
*Less intense green color and looked more reddish brown.
 +
 +
[[Image:2012-11-07_08.38.59.jpg|500px]]
 +
'''FTIR Results'''
'''FTIR Results'''
-
[[Image:1g22000PVOHcrosslinked.png]]
+
[[Image:1g22000PVOHcrosslinked.png|500px]]
 +
 
 +
 
 +
[[Image:1g22000PVOHH3PO4MaleicAcid.png|500px]]
 +
 
 +
[[Image:1g22000PVOHH3PO4MaleicAcidcrosslinked.png|500px]]
 +
 
 +
[[Image:1gPVOH22000H3PO4.png|500px]]
 +
 
 +
[[Image:1gPVOH100000.png|500px]]
 +
 
 +
[[Image:1gPVOH100000HCl.png|500px]]
 +
 
 +
[[Image:1gPVOH100000HClcrosslinked.png|500px]]
 +
 
 +
[[Image:Halfg22000PVOHgluteraldehyde.png|500px]]
 +
 
 +
[[Image:Halfg100000PVOHcrosslinked.png|500px]]
 +
 
 +
[[Image:HalfgPVOH2200.png|500px]]
 +
 
 +
[[Image:HalfgPVOH22000H3PO4.png|500px]]
 +
 
 +
[[Image:HalfgPVOH100000HCl.png|500px]]
 +
 
 +
[[Image:HalfgPVOH100000HClSuccinicAcid.png|500px]]
 +
 
 +
[[Image:OnetenthgPVOH22000.png|500px]]
 +
 
 +
[[Image:OnetenthgPVOH100000.png|500px]]
==Notes==
==Notes==

Current revision

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Objective

Description

Part 1

  • Place the porphyrin film (with 2 drops of HCL), prepared on 24/10/2012, into a 6 molality of NaCl with 100ml of HPLC water.
  • Place the NaCl solution in to a hot plate and wait until temperature raises to 70C.
  • At 70C place the film into beaker.


Part 2

  • FTIR measurement for every film that has been prepared.

Data

Porphyrin film with 2 drops of HCL, prepared on 24/10/2012

*Before cross-linking

  • The film shrunk and look more brittle.
  • More intense green color.

*After cross-linking

  • The film expanded a little.
  • Less intense green color and looked more reddish brown.


FTIR Results


Notes

This area is for any observations or conclusions that you would like to note.


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