User:Rebeca Rodriguez/Notebook/581/2014/09/19: Difference between revisions
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|style="background-color: #EEE"|[[Image: | |style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span> | ||
|style="background-color: #F2F2F2" align="center"| | |style="background-color: #F2F2F2" align="center"|[[File:Report.png|frameless|link={{#sub:{{FULLPAGENAME}}|0|-11}}]][[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|[[File:Resultset_previous.png|frameless|link={{#lnpreventry:{{FULLPAGENAME}}}}]][[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]] }}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]][[File:Resultset_next.png|frameless|link={{#lnnextentry:{{FULLPAGENAME}}}}]]}} | ||
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==Objective== | |||
# Start Analysis on pXRD spectra | |||
# new PVA and 10% PVA-clay synthesis | |||
# set up new experiments with PVA and PVA-clay films soaking in Arsenic (As) and Mercury (Hg) each with 150ppm, 100ppm, 50ppm | |||
==Protocol== | |||
====Synthesis of new films==== | |||
Synthesis is the same that was used on August 26th, 2014 | |||
<br> | |||
*10% PVA-Clay film | |||
1.0037g PVA and 0.1099g NaMT clay | |||
<br> | |||
*PVA film | |||
0.9998g PVA | |||
====PVA and PVA-clay in Hg and As==== | |||
Mass of films in each vial | |||
{| {{table}} | |||
| align="center" style="background:#f0f0f0;"|'''Vial #''' | |||
| align="center" style="background:#f0f0f0;"|'''Label''' | |||
| align="center" style="background:#f0f0f0;"|'''weight of vial and cap (g)''' | |||
| align="center" style="background:#f0f0f0;"|'''weight of vial, cap and film (g)''' | |||
| align="center" style="background:#f0f0f0;"|'''weight of film (g)''' | |||
|- | |||
| 1||PVA As 150ppm||16.4088||16.4996||0.0908 | |||
|- | |||
| 2||PVA As 100ppm||16.4369||16.5723||0.1354 | |||
|- | |||
| 3||PVA As 50ppm||16.4005||16.4869||0.0864 | |||
|- | |||
| 4||PVA Hg 150ppm||16.3721||16.4803||0.1082 | |||
|- | |||
| 5||PVA Hg 100 ppm||16.4145||16.5322||0.1177 | |||
|- | |||
| 6||PVA Hg 50 ppm||16.3643||16.489||0.1247 | |||
|- | |||
| 7||PVAC As 150ppm||16.3489||16.4425||0.0936 | |||
|- | |||
| 8||PVAC As 100ppm||16.4603||16.6209||0.1606 | |||
|- | |||
| 9||PVACAs 50ppm||16.4595||16.5439||0.0844 | |||
|- | |||
| 10||PVAC Hg 150 ppm||16.4208||16.5772||0.1564 | |||
|- | |||
| 11||PVAC Hg 100 ppm||16.4624||16.6448||0.1824 | |||
|- | |||
| 12||PVAC HG 50 ppm||16.3429||16.4028||0.0599 | |||
|} | |||
<br> | |||
Table of Solution Preparation | |||
{| {{table}} | |||
| align="center" style="background:#f0f0f0;"|'''Stock Solution (M)''' | |||
| align="center" style="background:#f0f0f0;"|'''0.0499''' | |||
|- | |||
| As stock solution (ppm) ||3738.61 | |||
|- | |||
| As 150ppm solution ||4mL stock in 100mL | |||
|- | |||
| As 100ppm Solution ||2.76mL stock in 100mL | |||
|- | |||
| As 50ppm solution||1.32mL stock in 100mL | |||
|- | |||
| Hg stock solution (ppm) ||268 | |||
|- | |||
| Hg 150ppm solution||13.99mL stock in 25mL | |||
|- | |||
| Hg 100ppm solution||9.32mL stock in 25mL | |||
|- | |||
| Hg 50ppm solution ||4.66mL stock in 25mL | |||
|} | |||
== | ====PVA-Clay Cation Exchange==== | ||
# After centrifugation the clay was laid out on a watch glass and dried | |||
# The dried clay was removed from glass and crushed using a mortar and pestle | |||
# It was then transferred into a scintillation vial and massed 1.0484g of NaMT cation exchange powder | |||
# The vial was placed into a oven in order to remove any excess hydrate | |||
==Data== | ==Data== | ||
====XRD analysis of PVA film soaked in 80ppm Malachite Green==== | |||
== | |||
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Latest revision as of 00:19, 27 September 2017
Project name | Main project page Previous entry Next entry | |||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||||
Objective
ProtocolSynthesis of new filmsSynthesis is the same that was used on August 26th, 2014
1.0037g PVA and 0.1099g NaMT clay
0.9998g PVA PVA and PVA-clay in Hg and AsMass of films in each vial
PVA-Clay Cation Exchange
DataXRD analysis of PVA film soaked in 80ppm Malachite Green |