User:Rebeca Rodriguez/Notebook/581/2014/09/12: Difference between revisions

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|style="background-color: #EEE"|[[Image:BDLlogo_notext_lr.png|128px]]<span style="font-size:22px;"> Biomaterials Design Lab</span>
|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span>
|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}}
|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}}
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==Objective==
==Objective==
Learn how to maintain an OpenWetWare Notebook.
*Prepare exfoliated clays
 
*Prepare new Malachite Green Solutions
==Description==
*Prepare samples for XRD analysis
# Add experimental record here. Include what, how, and why...
*get DSC data
 
==Data==
* Add data and results here...
 
==Notes==
This area is for any observations or conclusions that you would like to note.
 


Use categories like tags. Change the "Course" category to the one corresponding to your course. The "Miscellaneous" tag can be used for particular experiments, as instructed by your professor. Please be sure to change or delete this tag as required so that the categories remain well organized.


[[Category:Course]]
==Protocol==
[[Category:Miscellaneous]]
====Exfoliated Clays====
Use 1.0045g of PVA in 2.7701g NaMT in order to make the 10% clay film. Using the same protocol as August 27th, 2014.


====Powder Xray diffraction====
Prepared a PVA-film soaked in 80ppm Malachite Green for XRD analysis. We secured the film to the holder using tape and an XRD of the tape alone has been taken for comparison.


====Preparation of new Malachite Green (M.G.) solutions====
#200 ppm M.G. made by [[User:Madeleine Y. Bee/Notebook/CHEM-581 Experimental Chemistry/2014/09/12|Madeline Bee]] and calculations can be found on her page.
#80ppm M.G. made using 40mL of the 200ppm in 100mL volumetric flask.
#8ppm M.G. made by [[http://www.openwetware.org/wiki/User:Andrew_K_Farag/Notebook/CHEM-581/2014/09/12|Andrew Farag]] and calculations can be found on his page.
#2ppm M.G. made by [[http://openwetware.org/wiki/User:James_C._Schwabacher/Notebook/CHEM-571/2014/09/12|James Schwabacher]] calculations can be found on his page.


[[Category:Course]]
====Soaking PVA-Films in Malachite Green Solutions====
[[Category:Miscellaneous]]
*200 ppm M.G.
**Vial mass: 13.1452 g
**Vial + film mass: 13.2402 g
**Film mass: 0.095 g
*80 ppm M.G.
**Vial mass: 13.0894 g
**Vial + film mass: 13.1649 g
**Film mass: 0.0755 g
*8 ppm
**Vial mass: 12.9457 g
**Vial + film mass: 13.0512 g
**Film mass: 0.1055 g
*2 ppm
**Vial mass: 13.0611 g
**Vial + film mass: 13.1511 g
**Film mass: 0.09 g




Revision as of 16:10, 16 September 2014

Project name <html><img src="/images/9/94/Report.png" border="0" /></html> Main project page
<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>Previous entry<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>Next entry<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>

Objective

  • Prepare exfoliated clays
  • Prepare new Malachite Green Solutions
  • Prepare samples for XRD analysis
  • get DSC data


Protocol

Exfoliated Clays

Use 1.0045g of PVA in 2.7701g NaMT in order to make the 10% clay film. Using the same protocol as August 27th, 2014.

Powder Xray diffraction

Prepared a PVA-film soaked in 80ppm Malachite Green for XRD analysis. We secured the film to the holder using tape and an XRD of the tape alone has been taken for comparison.

Preparation of new Malachite Green (M.G.) solutions

  1. 200 ppm M.G. made by Madeline Bee and calculations can be found on her page.
  2. 80ppm M.G. made using 40mL of the 200ppm in 100mL volumetric flask.
  3. 8ppm M.G. made by [Farag] and calculations can be found on his page.
  4. 2ppm M.G. made by [Schwabacher] calculations can be found on his page.

Soaking PVA-Films in Malachite Green Solutions

  • 200 ppm M.G.
    • Vial mass: 13.1452 g
    • Vial + film mass: 13.2402 g
    • Film mass: 0.095 g
  • 80 ppm M.G.
    • Vial mass: 13.0894 g
    • Vial + film mass: 13.1649 g
    • Film mass: 0.0755 g
  • 8 ppm
    • Vial mass: 12.9457 g
    • Vial + film mass: 13.0512 g
    • Film mass: 0.1055 g
  • 2 ppm
    • Vial mass: 13.0611 g
    • Vial + film mass: 13.1511 g
    • Film mass: 0.09 g




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