User:Rebeca Rodriguez/Notebook/581/2014/09/12: Difference between revisions

From OpenWetWare
< User:Rebeca Rodriguez‎ | Notebook‎ | 581‎ | 2014‎ | 09
Jump to navigationJump to search
(Autocreate 2014/09/12 Entry for User:Rebeca_Rodriguez/Notebook/581)
 
(fix raw html notebook nav)
 
(One intermediate revision by one other user not shown)
Line 1: Line 1:
{|{{table}} width="800"
{|{{table}} width="800"
|-
|-
|style="background-color: #EEE"|[[Image:BDLlogo_notext_lr.png|128px]]<span style="font-size:22px;"> Biomaterials Design Lab</span>
|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span>
|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}}
|style="background-color: #F2F2F2" align="center"|[[File:Report.png|frameless|link={{#sub:{{FULLPAGENAME}}|0|-11}}]][[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|[[File:Resultset_previous.png|frameless|link={{#lnpreventry:{{FULLPAGENAME}}}}]][[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]][[File:Resultset_next.png|frameless|link={{#lnnextentry:{{FULLPAGENAME}}}}]]}}
|-
|-
| colspan="2"|
| colspan="2"|
<!-- ##### DO NOT edit above this line unless you know what you are doing. ##### -->
<!-- ##### DO NOT edit above this line unless you know what you are doing. ##### -->
==Objective==
==Objective==
Learn how to maintain an OpenWetWare Notebook.
*Prepare exfoliated clays
 
*Prepare new Malachite Green Solutions
==Description==
*Prepare samples for XRD analysis
# Add experimental record here. Include what, how, and why...
*get DSC data
 
==Data==
* Add data and results here...
 
==Notes==
This area is for any observations or conclusions that you would like to note.
 


Use categories like tags. Change the "Course" category to the one corresponding to your course. The "Miscellaneous" tag can be used for particular experiments, as instructed by your professor. Please be sure to change or delete this tag as required so that the categories remain well organized.


[[Category:Course]]
==Protocol==
[[Category:Miscellaneous]]
====Exfoliated Clays====
Use 1.0045g of PVA in 2.7701g NaMT in order to make the 10% clay film. Using the same protocol as August 27th, 2014.


====Powder Xray diffraction====
Prepared a PVA-film soaked in 80ppm Malachite Green for XRD analysis. We secured the film to the holder using tape and an XRD of the tape alone has been taken for comparison.


====Preparation of new Malachite Green (M.G.) solutions====
#200 ppm M.G. made by [[User:Madeleine Y. Bee/Notebook/CHEM-581 Experimental Chemistry/2014/09/12|Madeline Bee]] and calculations can be found on her page.
#80ppm M.G. made using 40mL of the 200ppm in 100mL volumetric flask.
#8ppm M.G. made by [[http://www.openwetware.org/wiki/User:Andrew_K_Farag/Notebook/CHEM-581/2014/09/12|Andrew Farag]] and calculations can be found on his page.
#2ppm M.G. made by [[http://openwetware.org/wiki/User:James_C._Schwabacher/Notebook/CHEM-571/2014/09/12|James Schwabacher]] calculations can be found on his page.


[[Category:Course]]
====Soaking PVA-Films in Malachite Green Solutions====
[[Category:Miscellaneous]]
*200 ppm M.G.
**Vial mass: 13.1452 g
**Vial + film mass: 13.2402 g
**Film mass: 0.095 g
*80 ppm M.G.
**Vial mass: 13.0894 g
**Vial + film mass: 13.1649 g
**Film mass: 0.0755 g
*8 ppm
**Vial mass: 12.9457 g
**Vial + film mass: 13.0512 g
**Film mass: 0.1055 g
*2 ppm
**Vial mass: 13.0611 g
**Vial + film mass: 13.1511 g
**Film mass: 0.09 g




Latest revision as of 00:17, 27 September 2017

Project name Main project page
Previous entry      Next entry

Objective

  • Prepare exfoliated clays
  • Prepare new Malachite Green Solutions
  • Prepare samples for XRD analysis
  • get DSC data


Protocol

Exfoliated Clays

Use 1.0045g of PVA in 2.7701g NaMT in order to make the 10% clay film. Using the same protocol as August 27th, 2014.

Powder Xray diffraction

Prepared a PVA-film soaked in 80ppm Malachite Green for XRD analysis. We secured the film to the holder using tape and an XRD of the tape alone has been taken for comparison.

Preparation of new Malachite Green (M.G.) solutions

  1. 200 ppm M.G. made by Madeline Bee and calculations can be found on her page.
  2. 80ppm M.G. made using 40mL of the 200ppm in 100mL volumetric flask.
  3. 8ppm M.G. made by [Farag] and calculations can be found on his page.
  4. 2ppm M.G. made by [Schwabacher] calculations can be found on his page.

Soaking PVA-Films in Malachite Green Solutions

  • 200 ppm M.G.
    • Vial mass: 13.1452 g
    • Vial + film mass: 13.2402 g
    • Film mass: 0.095 g
  • 80 ppm M.G.
    • Vial mass: 13.0894 g
    • Vial + film mass: 13.1649 g
    • Film mass: 0.0755 g
  • 8 ppm
    • Vial mass: 12.9457 g
    • Vial + film mass: 13.0512 g
    • Film mass: 0.1055 g
  • 2 ppm
    • Vial mass: 13.0611 g
    • Vial + film mass: 13.1511 g
    • Film mass: 0.09 g




Retrieved from "https://openwetware.org/mediawiki/index.php?title=User:Rebeca_Rodriguez/Notebook/581/2014/09/12&oldid=1015327"