User:Paul Rothenberg/Notebook/Pauls Notebook/2013/06/10: Difference between revisions
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== | ==Reaction of OPD+H<sub>2</sub>O<sub>2</sub> with Mb/Citrate Catalyst in Acetonitrile Suspension== | ||
Instead of running this reaction in the previous fashion, we are going to try to run this in a beaker with a stir bar to prevent the reaction tube to be shaken every few minutes. We will also filter the solution before taking a spectrum. We will follow the same [http://openwetware.org/wiki/User:Paul_Rothenberg/Notebook/Pauls_Notebook/2013/05/31 procedure] as with the Isopropanol suspension and the previous acetonitrile suspensions. | |||
<b>10:05:</b> The reaction was started. Samples were removed every 20 minutes and pushed through a syringe filter directly into the cuvette. 7 samples total were taken and analyzed. | |||
<b>Data:</b> | |||
[[Image:Mb_Citrate_OPD_H2O2_MeCN_FILTERED_WORKUP_GRAPH.png|750px]] | |||
== Reaction of OPD+H<sub>2</sub>O<sub>2</sub> with Mb/Phosphate Catalyst in Acetonitrile Suspension == | |||
<b>Data:</b> | |||
[[Image:Mb_Phosphate_OPD_H2O2_MeCN_FILTERED_WORKUP_GRAPH.png|750px]] | |||
== Reaction of OPD+H<sub>2</sub>O<sub>2</sub> with Mb/Acetate Catalyst in Acetonitrile Suspension == | |||
<b>Data:</b> | |||
[[Image:Mb_Acetate_OPD_H2O2_MeCN_FILTERED_WORKUP_GRAPH.png|750px]] | |||
Revision as of 09:28, 8 July 2013
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Reaction of OPD+H2O2 with Mb/Citrate Catalyst in Acetonitrile SuspensionInstead of running this reaction in the previous fashion, we are going to try to run this in a beaker with a stir bar to prevent the reaction tube to be shaken every few minutes. We will also filter the solution before taking a spectrum. We will follow the same procedure as with the Isopropanol suspension and the previous acetonitrile suspensions. 10:05: The reaction was started. Samples were removed every 20 minutes and pushed through a syringe filter directly into the cuvette. 7 samples total were taken and analyzed. Data:
Reaction of OPD+H2O2 with Mb/Phosphate Catalyst in Acetonitrile SuspensionData:
Reaction of OPD+H2O2 with Mb/Acetate Catalyst in Acetonitrile SuspensionData:
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