User:Paul Rothenberg/Notebook/Pauls Notebook/2013/06/10: Difference between revisions

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==Reaction of OPD+H<sub>2</sub>O<sub>2</sub> with Mb/Citrate Catalyst in Acetonitrile Suspension==
==Reaction of OPD+H<sub>2</sub>O<sub>2</sub> with Mb/Citrate Catalyst in Acetonitrile Suspension==
* Instead of running this reaction in the previous fashion, we are going to try to run this in a beaker with a stir bar to prevent the reaction tube to be shaken every few minutes. We will also filter the solution before taking a spectrum. We will follow the same [http://openwetware.org/wiki/User:Paul_Rothenberg/Notebook/Pauls_Notebook/2013/05/31 procedure] as with the Isopropanol suspension and the previous acetonitrile suspensions.  
* Instead of running this reaction in the previous fashion, we are going to try to run this in a beaker with a stir bar to prevent the reaction tube to be shaken every few minutes. We will also filter the solution before taking a spectrum. We will follow the same [http://openwetware.org/wiki/User:Paul_Rothenberg/Notebook/Pauls_Notebook/2013/05/31 procedure] as with the Isopropanol suspension and the previous acetonitrile suspensions.  
<b>10:05:</b> The reaction was started. Samples were removed every 20 minutes and pushed through a syringe filter directly into the cuvette.





Revision as of 08:29, 10 June 2013

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Reaction of OPD+H2O2 with Mb/Citrate Catalyst in Acetonitrile Suspension

  • Instead of running this reaction in the previous fashion, we are going to try to run this in a beaker with a stir bar to prevent the reaction tube to be shaken every few minutes. We will also filter the solution before taking a spectrum. We will follow the same procedure as with the Isopropanol suspension and the previous acetonitrile suspensions.

10:05: The reaction was started. Samples were removed every 20 minutes and pushed through a syringe filter directly into the cuvette.