User:Moira M. Esson/Notebook/CHEM-581/2013/04/12: Difference between revisions

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# Run X-ray on prepared microspheres with a 50:50 ratio of PVA/clay.
# Run X-ray on prepared microspheres with a 50:50 ratio of PVA/clay.
# Add deionized H<sub>2</sub>O to all prepared hydrogels in preparation for DSC.
# Add deionized H<sub>2</sub>O to all prepared hydrogels in preparation for DSC.
# View prepared microspheres under microscope.
<br>
==DSC==
* The general protocol for DSC was used
* Specific DSC parameters and protocols set to analyze PVA/clay samples were:
    # Equilibrate sample at ~ -40°C
    # Ramp sample temperature up from 20-240°C
    # Ramp sample temperature down from 20-(-40°C)
    # Repeat segment #2 again
<br>
Table 1. DSC sample preparation
<br>
{| {{table}}
| align="center" style="background:#f0f0f0;"|'''Sample Name'''
| align="center" style="background:#f0f0f0;"|'''Sample Mass (mg)'''
| align="center" style="background:#f0f0f0;"|'''Pan / Lid Mass (mg)'''
|-
| 90:10 PVOH 146K 50% CEC NaMT w/ Bu<sub>3</sub>HdP<sup>+</sup>||3.10||49.78
|-
| 90:10 PVOH 146K NaMT||3.01||49.99
|}
<br>
==Film Preparation==




Revision as of 06:50, 15 April 2013

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Objectives

  1. Finish PVA/clay film preparation.
  2. Finish preparing DSC samples.
  3. Run DSC.
  4. Run X-ray on prepared microspheres with a 50:50 ratio of PVA/clay.
  5. Add deionized H2O to all prepared hydrogels in preparation for DSC.
  6. View prepared microspheres under microscope.


DSC

  • The general protocol for DSC was used
  • Specific DSC parameters and protocols set to analyze PVA/clay samples were:
   # Equilibrate sample at ~ -40°C
   # Ramp sample temperature up from 20-240°C
   # Ramp sample temperature down from 20-(-40°C)
   # Repeat segment #2 again


Table 1. DSC sample preparation

Sample Name Sample Mass (mg) Pan / Lid Mass (mg)
90:10 PVOH 146K 50% CEC NaMT w/ Bu3HdP+ 3.10 49.78
90:10 PVOH 146K NaMT 3.01 49.99


Film Preparation


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