User:Moira M. Esson/Notebook/CHEM-581/2013/04/12: Difference between revisions
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*The general protocol for film preparation described on [[User:Moira_M._Esson/Notebook/CHEM-581/2012/08/29|2012/08/29]] was followed. The necessary amount of clay was added in the correct ratio. All films were prepared on a 0.5g scale. The films were placed in a freezer at -20°C immediately after pouring. These films will undergo the cyclic freeze-thaw procedure used for hydrogel preparation. | *The general protocol for film preparation described on [[User:Moira_M._Esson/Notebook/CHEM-581/2012/08/29|2012/08/29]] was followed. The necessary amount of clay was added in the correct ratio. All films were prepared on a 0.5g scale. The films were placed in a freezer at -20°C immediately after pouring. These films will undergo the cyclic freeze-thaw procedure used for hydrogel preparation. | ||
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Table | Table 2. Film Preparation | ||
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Revision as of 10:12, 15 April 2013
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Objectives
DSC
# Equilibrate sample at ~ -40°C # Ramp sample temperature up from 20-240°C # Ramp sample temperature down from 20-(-40°C) # Repeat segment #2 again
Film Preparation
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