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Objectives
- Perform polyvinyl acetate synthesis
- ISE film preparation(do this for film selectivity)
ISE film preparation
General Protocol
- Cut PVOH film in half. Place each half in a 100mL beaker. There will be two beakers used for each film.
- Fill one beaker with ~50mL 20ppm CuSO4 stock solution. Make sure enough solution is used to completely cover the film.
- Fill the second beaker with ~50mL 20ppm NaSO4 stock solution. Make sure enough solution is used to completely cover the film.
- Allow the films to sit for ~48hours
Notes:
- The films that were used were PVOH(MW 22K)+0.8wt% GA crosslinked and PVOH(MW 22K)+0.8wt% GA+NaMT crosslinked
Acetylation
- The general protocol for acetylation described [[Category:]]
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