User:Moira M. Esson/Notebook/CHEM-581/2012/11/14 - Revision history

Moira M. Esson: /* Acetylation */

Moira M. Esson — Fri, 30 Nov 2012 19:02:25 GMT

Acetylation

←Older revision		Revision as of 19:02, 30 November 2012
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	\| align="center" style="background:#f0f0f0;"\|'''Total volume used(mL)'''		\| align="center" style="background:#f0f0f0;"\|'''Total volume used(mL)'''
	\|-		\|-
-	\| 20%\|\|\|\|\|\|	+	\| 20%\|\|0.5\|\|42.5\|\|42
	\|-		\|-
-	\| 40%\|\|\|\|\|\|	+	\| 40%\|\|0.0\|\|43.2\|\|43.2
	\|-		\|-
-	\| 60%\|\|\|\|\|\|	+	\| 60%\|\|0.1\|\|42.8\|\|42.7
	\|}		\|}

Moira M. Esson: /* Acetylation */

Moira M. Esson — Mon, 26 Nov 2012 22:09:43 GMT

Acetylation

←Older revision		Revision as of 22:09, 26 November 2012
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	<br>		<br>
	==Acetylation==		==Acetylation==
-	*The general protocol for acetylation described [[~~Category~~:]]	+	*The general protocol for acetylation described [[User:Moira_M._Esson/Notebook/CHEM-581/2012/11/09\|2012/11/09]] was used.
		+	*Three reaction mixtures(20%, 40% and 60%) were placed on a stir plate for 1 hour.
		+	Note:
		+	*Three drops of bromothymol blue were added to each reaction mixture before titrating with sodium bicarbonate solution prepared [[User:Moira_M._Esson/Notebook/CHEM-581/2012/11/09\|2012/11/09]]
		+	*PHP solution had not completely dissolved. Standardization of sodium bicarbonate must still be performed. In order to facilitate the dissolving of PHP, 20.424g of PHP will be remeasured, dried and divided three equivalent portions. These equivalent portions will be added to three separate beakers and deionized H<sub>2</sub>O will be added to the beakers to create a 1M solution.
		+	Titration results:
		+	{\| {{table}}
		+	\| align="center" style="background:#f0f0f0;"\|'''Reaction mixture'''
		+	\| align="center" style="background:#f0f0f0;"\|'''Initial volume of burette(mL)'''
		+	\| align="center" style="background:#f0f0f0;"\|'''Final volume burette(mL)'''
		+	\| align="center" style="background:#f0f0f0;"\|'''Total volume used(mL)'''
		+	\|-
		+	\| 20%\|\|\|\|\|\|
		+	\|-
		+	\| 40%\|\|\|\|\|\|
		+	\|-
		+	\| 60%\|\|\|\|\|\|
		+	\|}

Moira M. Esson: /* Entry title */

Moira M. Esson — Mon, 26 Nov 2012 21:56:51 GMT

Entry title

←Older revision		Revision as of 21:56, 26 November 2012
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	\| colspan="2"\|		\| colspan="2"\|
	<!-- ##### DO NOT edit above this line unless you know what you are doing. ##### -->		<!-- ##### DO NOT edit above this line unless you know what you are doing. ##### -->
-	==~~Entry title~~==	+	==Objectives==
-	* Insert content here...	+	#Perform polyvinyl acetate synthesis
		+	#ISE film preparation(do this for film selectivity)
		+	==ISE film preparation==
		+	General Protocol
		+	#Cut PVOH film in half. Place each half in a 100mL beaker. There will be two beakers used for each film.
		+	#Fill one beaker with ~50mL 20ppm CuSO<sub>4</sub> stock solution. Make sure enough solution is used to completely cover the film.
		+	#Fill the second beaker with ~50mL 20ppm NaSO<sub>4</sub> stock solution. Make sure enough solution is used to completely cover the film.
		+	#Allow the films to sit for ~48hours
		+	Notes:
		+	*The films that were used were PVOH(MW 22K)+0.8wt% GA crosslinked and PVOH(MW 22K)+0.8wt% GA+NaMT crosslinked
		+	<br>
		+	==Acetylation==
		+	*The general protocol for acetylation described [[Category:]]
		+
		+

Moira M. Esson: Autocreate 2012/11/14 Entry for User:Moira_M._Esson/Notebook/CHEM-581

Moira M. Esson — Mon, 26 Nov 2012 21:44:14 GMT

Autocreate 2012/11/14 Entry for User:Moira_M._Esson/Notebook/CHEM-581

New page

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|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html>      </html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}}
|-
| colspan="2"|

==Entry title==
* Insert content here...


|}

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