User:Moira M. Esson/Notebook/CHEM-581/2012/10/26

(Difference between revisions)

Revision as of 18:15, 10 November 2012

Project name

Crosslink porphyrin films
Run AA using film adsorption
Prepare next highest porphyrin concentration solution. Then add salts to these higher porphyrin solutions
Run UV-vis on film adsorption and porphyrin-salt solutions

The general protocol for porphyrin film crosslinking described on 2012/09/14 was followed for the films listed below

Films Crosslinked:

Crosslinking information

Films	Amount of fixant solution used to crosslink(mL)	Amount fixant solution kept in vial(mL)	Amount of 1% aqueous HCl solution used to crosslink(mL	Amount HCl solution saved in vial(mL)	Amount of 0.2M sodium bicarbonate used(mL)	Amount sodium bicarbonate solution saved(mL)
PVOH(22K) 1.0073g+1.0mL GA+1mL porphyrin	99.95	13	100	14	100	12
PVOH(22K) 1.05225g+1.0mL GA+1mL porphyrin	101	12	98	13	99.8	12

@@ Line 23: / Line 23: @@
 | align="center" style="background:#f0f0f0;"|'''Films'''
 | align="center" style="background:#f0f0f0;"|'''Amount of fixant solution used to crosslink(mL)'''
-| align="center" style="background:#f0f0f0;"|''''''
-| align="center" style="background:#f0f0f0;"|''''''
-| align="center" style="background:#f0f0f0;"|''''''
 | align="center" style="background:#f0f0f0;"|'''Amount fixant solution kept in vial(mL)'''
 | align="center" style="background:#f0f0f0;"|'''Amount of 1% aqueous HCl solution used to crosslink(mL'''
@@ Line 32: / Line 29: @@
 | align="center" style="background:#f0f0f0;"|'''Amount sodium bicarbonate solution saved(mL)'''
 |-
-| PVOH(22K) 1.0073g+1.0mL GA+1mL porphyrin||99.95||||||||13||100||14||100||12
+| PVOH(22K) 1.0073g+1.0mL GA+1mL porphyrin||99.95||13||100||14||100||12
 |-
-| PVOH(22K) 1.05225g+1.0mL GA+1mL porphyrin||101||||||||12||98||13||99.8||12
+| PVOH(22K) 1.05225g+1.0mL GA+1mL porphyrin||101||12||98||13||99.8||12
 |}