User:Mobeen Ashraf/Notebook/Chem-581/2012/11/02

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(Objective)
(Objective)
Line 14: Line 14:
* Adsorption through films similar to clay films instead of clay :
* Adsorption through films similar to clay films instead of clay :
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-1.04 g Fe(II) Cl, 0.5 g Iron Sulfate, 1 film, and 40 ml H2O.  
+
**1.04 g Fe(II) Cl, 0.5 g Iron Sulfate, 1 film, and 40 ml H2O.  
-
-To precipitate iron oxide out of the solution NaOH ( 2.67 g in 10 ml H2O) was added drop wise with stirring.  
+
**To precipitate iron oxide out of the solution NaOH ( 2.67 g in 10 ml H2O) was added drop wise with stirring.  
-
_ The solution was then filtered using vacuum filtration and left to dry.  
+
**The solution was then filtered using vacuum filtration and left to dry.  
* Add film with Porphyrin and glutaraldehyde to 1% solution of HCl and leave out until the next working day.
* Add film with Porphyrin and glutaraldehyde to 1% solution of HCl and leave out until the next working day.

Revision as of 15:18, 28 November 2012

Experimental Chemistry Main project page
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Objective

  • Make 1:1 ratio of sulfate ions solution ( H2SO4, Fe2(SO4)3, FeSO4, Na2SO4, Al2(SO4)3).
  • Adsorption through films similar to clay films instead of clay :
    • 1.04 g Fe(II) Cl, 0.5 g Iron Sulfate, 1 film, and 40 ml H2O.
    • To precipitate iron oxide out of the solution NaOH ( 2.67 g in 10 ml H2O) was added drop wise with stirring.
    • The solution was then filtered using vacuum filtration and left to dry.
  • Add film with Porphyrin and glutaraldehyde to 1% solution of HCl and leave out until the next working day.

Description

  • 3 PVOH films were prepared: 0.5 g MW of 22,000, 1 ml glutaraldehyde, and 1 ml of porphrine dihydrogen chloride.
  • AAS studies for all the Cu standards: NaMT- concentration of 1.25 g/500 ml, for 1min, 5 min and 10 mins standards, 50 % CEC exchange-concentration of 1.25 g/500 ml, for 1 min, 5 min and 10 mins standards, 100% CEC exchange, for 1 min, 5 min and 10 mins standards, and Fe3O4-concentration of 1.25 g/500 ml, for 1 min, 5 min and 10 mins standards.

Data

  • Add data and results here...

Notes

This area is for any observations or conclusions that you would like to note.


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