User:Melissa Novy/Notebook/CHEM-581/2012/10/31 - Revision history

Melissa Novy: /* Objectives */

2012-11-30T19:00:31Z

Objectives

←Older revision		Revision as of 19:00, 30 November 2012
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	==Objectives==		==Objectives==
	* Analyze all films made since 2012/08/31 with FTIR.		* Analyze all films made since 2012/08/31 with FTIR.
		+	** Please refer to [[User:Moira_M._Esson/Notebook/CHEM-581/2012/11/05\|Moira Esson's entry]] for a list of films analyzed.
	* Make a film of PVOH (MW 22000) and 5-hydroxymethyl(furfural) with HCl.		* Make a film of PVOH (MW 22000) and 5-hydroxymethyl(furfural) with HCl.
	* Make more concentrated porphine solutions with Al<sup>+3</sup>, Fe<sup>+3</sup>, or Na<sup>+2</sup> salts for UV-vis analysis.		* Make more concentrated porphine solutions with Al<sup>+3</sup>, Fe<sup>+3</sup>, or Na<sup>+2</sup> salts for UV-vis analysis.

Melissa Novy: /* Objectives */

2012-11-30T18:57:39Z

Objectives

←Older revision		Revision as of 18:57, 30 November 2012
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	* Make more concentrated porphine solutions with Al<sup>+3</sup>, Fe<sup>+3</sup>, or Na<sup>+2</sup> salts for UV-vis analysis.		* Make more concentrated porphine solutions with Al<sup>+3</sup>, Fe<sup>+3</sup>, or Na<sup>+2</sup> salts for UV-vis analysis.
	* Conduct ion diffusion analysis on PVOH(22K) + 1 mL GA films exchanged for 10 min with CuSO<sub>4</sub>.		* Conduct ion diffusion analysis on PVOH(22K) + 1 mL GA films exchanged for 10 min with CuSO<sub>4</sub>.
		+
		+	==PVOH(22K) + Furfural Film==
		+	* Please refer to [[User:Karlena_L._Brown/Notebook/PVOH_Research/2012/10/31\|Karlena Brown's entry]] for the protocol and observations.

	==Ion Diffusion Analysis==		==Ion Diffusion Analysis==

Melissa Novy: /* Ion Diffusion Analysis */

2012-11-30T18:42:54Z

Ion Diffusion Analysis

←Older revision		Revision as of 18:42, 30 November 2012
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	==Ion Diffusion Analysis==		==Ion Diffusion Analysis==
-	* Please refer to [[User:Karlena_L._Brown/Notebook/PVOH_Research/2012/10/31\|Karlena Brown's entry]] for the ISE conductivity protocol.	+	* Please refer to [[User:Karlena_L._Brown/Notebook/PVOH_Research/2012/10/31\|Karlena Brown's entry]] for the ISE conductivity protocol and observations.
	** Note that the varied ion solution contained 1000 ppm each of Cl<sup>-</sup>, Br<sup>-</sup>, and I<sup>-</sup>.		** Note that the varied ion solution contained 1000 ppm each of Cl<sup>-</sup>, Br<sup>-</sup>, and I<sup>-</sup>.
	<br>		<br>

Melissa Novy: /* Objectives */

2012-11-30T18:42:24Z

Objectives

←Older revision		Revision as of 18:42, 30 November 2012
Line 18:		Line 18:
	* Make a film of PVOH (MW 22000) and 5-hydroxymethyl(furfural) with HCl.		* Make a film of PVOH (MW 22000) and 5-hydroxymethyl(furfural) with HCl.
	* Make more concentrated porphine solutions with Al<sup>+3</sup>, Fe<sup>+3</sup>, or Na<sup>+2</sup> salts for UV-vis analysis.		* Make more concentrated porphine solutions with Al<sup>+3</sup>, Fe<sup>+3</sup>, or Na<sup>+2</sup> salts for UV-vis analysis.
		+	* Conduct ion diffusion analysis on PVOH(22K) + 1 mL GA films exchanged for 10 min with CuSO<sub>4</sub>.

		+	==Ion Diffusion Analysis==
		+	* Please refer to [[User:Karlena_L._Brown/Notebook/PVOH_Research/2012/10/31\|Karlena Brown's entry]] for the ISE conductivity protocol.
		+	** Note that the varied ion solution contained 1000 ppm each of Cl<sup>-</sup>, Br<sup>-</sup>, and I<sup>-</sup>.
		+	<br>
		+	HPLC-Grade H<sub>2</sub>O Solution
		+	{\| {{table}}
		+	\| align="center" style="background:#f0f0f0;"\|'''Time Recordings'''
		+	\| align="center" style="background:#f0f0f0;"\|'''Initial Volume[mL]'''
		+	\| align="center" style="background:#f0f0f0;"\|'''Final Volume [mL]'''
		+	\| align="center" style="background:#f0f0f0;"\|'''Conductivity [μS/cm]'''
		+	\|-
		+	\| 8:50AM\|\|28\|\|28\|\|19.93
		+	\|-
		+	\| 9:00AM\|\|28\|\|29\|\|23.13
		+	\|-
		+	\| 9:30AM\|\|29\|\|29\|\|24.60
		+	\|-
		+	\| 10:00AM\|\|29\|\|28.5\|\|27.20
		+	\|-
		+	\| 10:30AM\|\|28.5\|\|29\|\|30.5
		+	\|-
		+	\| 11:00AM\|\|29\|\|29\|\|33
		+	\|-
		+	\| 11:30AM\|\|29\|\|29\|\|35.7
		+	\|-
		+	\| 12:00PM\|\|29\|\|29\|\|38.9
		+	\|-
		+	\| 3:15PM\|\|29\|\|28.6\|\|52.7
		+	\|-
		+	\| 9:00PM\|\|28.6\|\|27.2\|\|76.2
		+	\|}
		+	<br>
		+	Varied Ion Solution
		+	{\| {{table}}
		+	\| align="center" style="background:#f0f0f0;"\|'''Time Recordings'''
		+	\| align="center" style="background:#f0f0f0;"\|'''Initial Volume(mL)'''
		+	\| align="center" style="background:#f0f0f0;"\|'''Final Volume (mL)'''
		+	\| align="center" style="background:#f0f0f0;"\|'''Conductivity (μS/cm)'''
		+	\|-
		+	\| 8:50AM\|\|30\|\|30\|\|864
		+	\|-
		+	\| 9:00AM\|\|30\|\|30\|\|869
		+	\|-
		+	\| 9:30AM\|\|30\|\|30\|\|874
		+	\|-
		+	\| 10:00AM\|\|30\|\|30\|\|865
		+	\|-
		+	\| 10:30AM\|\|30\|\|30\|\|863
		+	\|-
		+	\| 11:00AM\|\|30\|\|29.5\|\|861
		+	\|-
		+	\| 11:30AM\|\|29.5\|\|30\|\|858
		+	\|-
		+	\| 12:00PM\|\|30\|\|30\|\|853
		+	\|-
		+	\| 3:15PM\|\|30\|\|29.8\|\|840
		+	\|-
		+	\| 9:00PM\|\|29.8\|\|28\|\|819
		+	\|}

	<!-- ##### DO NOT edit below this line unless you know what you are doing. ##### -->		<!-- ##### DO NOT edit below this line unless you know what you are doing. ##### -->

Melissa Novy: /* Objectives */

2012-10-31T19:07:14Z

Objectives

←Older revision		Revision as of 19:07, 31 October 2012
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	<!-- ##### DO NOT edit above this line unless you know what you are doing. ##### -->		<!-- ##### DO NOT edit above this line unless you know what you are doing. ##### -->
	==Objectives==		==Objectives==
-	* Analyze all films made since 2012/09/ with FTIR.	+	* Analyze all films made since 2012/08/31 with FTIR.
	* Make a film of PVOH (MW 22000) and 5-hydroxymethyl(furfural) with HCl.		* Make a film of PVOH (MW 22000) and 5-hydroxymethyl(furfural) with HCl.
	* Make more concentrated porphine solutions with Al<sup>+3</sup>, Fe<sup>+3</sup>, or Na<sup>+2</sup> salts for UV-vis analysis.		* Make more concentrated porphine solutions with Al<sup>+3</sup>, Fe<sup>+3</sup>, or Na<sup>+2</sup> salts for UV-vis analysis.

Melissa Novy at 19:06, 31 October 2012

2012-10-31T19:06:20Z

←Older revision		Revision as of 19:06, 31 October 2012
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	<!-- ##### DO NOT edit above this line unless you know what you are doing. ##### -->		<!-- ##### DO NOT edit above this line unless you know what you are doing. ##### -->
-	==~~Entry title~~==	+	==Objectives==
-	* ~~Insert content here~~...	+	* Analyze all films made since 2012/09/ with FTIR.
		+	* Make a film of PVOH (MW 22000) and 5-hydroxymethyl(furfural) with HCl.
		+	* Make more concentrated porphine solutions with Al<sup>+3</sup>, Fe<sup>+3</sup>, or Na<sup>+2</sup> salts for UV-vis analysis.

Melissa Novy: Autocreate 2012/10/31 Entry for User:Melissa_Novy/Notebook/CHEM-581

2012-10-31T19:04:30Z

Autocreate 2012/10/31 Entry for User:Melissa_Novy/Notebook/CHEM-581

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