User:Melissa Novy/Notebook/CHEM-572/2013/04/03

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(Autocreate 2013/04/03 Entry for User:Melissa_Novy/Notebook/CHEM-572)
Current revision (14:27, 10 April 2013) (view source)
 
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==Entry title==
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==Objectives==
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* Insert content here...
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* Filter more 100AgLMT.
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* Make films of PLA2002D + 33wt% LMT and PLA2002D + 33wt% 100AgLMT.
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==100AgLMT==
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* The reserved gel of 100AgLMT, made on [[User:Melissa_Novy/Notebook/CHEM-572/2013/02/12|2013/02/12]], was filtered with 42 Whatman paper and washed with 3 10-mL aliquots of (50:50) H<sub>2</sub>O/EtOH.  Afterward, the clay was placed in an aluminum dish in an 80°C oven to dry overnight.  It was subsequently ground with a mortar and pestle for use in films.
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==PLA2002D Films==
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* The protocol on [[User:Melissa_Novy/Notebook/CHEM-572/2013/02/06|2013/02/06]] was followed to make both films.
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<br>
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PLA2002D + 33wt% LMT
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* Theoretical mass PLA2002D: 3.00 g
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** Actual mass PLA2002D: 3.01 g
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* Theoretical mass LMT: 1.02206 g
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** Actual mass LMT: 1.00121 g
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<br>
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PLA2002D + 33wt% 100AgLMT
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* Theoretical mass PLA2002D: 3.00 g
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** Actual mass PLA2002D: 3.00 g
 +
* Theoretical mass 100AgLMT: 1.02206 g
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** Actual mass 100AgLMT: 0.52178 g
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<br>
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* Note that there was not enough 100AgLMT remaining to achieve 1.02206 g of sample. The final amount of 100AgLMT in the film was 17% of the 3 g of polymer.

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Objectives

  • Filter more 100AgLMT.
  • Make films of PLA2002D + 33wt% LMT and PLA2002D + 33wt% 100AgLMT.

100AgLMT

  • The reserved gel of 100AgLMT, made on 2013/02/12, was filtered with 42 Whatman paper and washed with 3 10-mL aliquots of (50:50) H2O/EtOH. Afterward, the clay was placed in an aluminum dish in an 80°C oven to dry overnight. It was subsequently ground with a mortar and pestle for use in films.

PLA2002D Films

  • The protocol on 2013/02/06 was followed to make both films.


PLA2002D + 33wt% LMT

  • Theoretical mass PLA2002D: 3.00 g
    • Actual mass PLA2002D: 3.01 g
  • Theoretical mass LMT: 1.02206 g
    • Actual mass LMT: 1.00121 g


PLA2002D + 33wt% 100AgLMT

  • Theoretical mass PLA2002D: 3.00 g
    • Actual mass PLA2002D: 3.00 g
  • Theoretical mass 100AgLMT: 1.02206 g
    • Actual mass 100AgLMT: 0.52178 g


  • Note that there was not enough 100AgLMT remaining to achieve 1.02206 g of sample. The final amount of 100AgLMT in the film was 17% of the 3 g of polymer.



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