User:Melissa Novy/Notebook/CHEM-572/2013/01/30/2013/02/05
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| + | ==Objectives== | ||
| + | * Analyze LMT-95Ag with X-ray diffraction. | ||
| + | * Analyze LMT-95Ag filtrate with silver ion-selective electrode. | ||
| + | * Begin ion exchange reaction with AgNO<sub>3</sub> and LMT to obtain LMT-100Ag. | ||
| + | ==Calculations== | ||
| + | '''MW AgNO<sub>3</sub>: 169.87 g/mol''' | ||
| + | '''MW Ag<sup>+</sup>: 107.86 g/mol''' | ||
| + | '''CEC Laponite: 55 meqv/100 g''' | ||
| + | '''1.5 g LMT × (55 meqv/100 g LMT) × (1 mol Ag<sup>+</sup>/1000 meqv) × (107.86 g Ag<sup>+</sup>/1 mol Ag<sup>+</sup>) × (1 mol Ag<sup>+</sup>/1 mol AgNO<sub>3</sub>) × (1 mol AgNO<sub>3</sub>/169.87 g AgNO<sub>3</sub>) × 100% = 0.000524 g AgNO<sub>3</sub>''' | ||
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| + | ==Laponite-Ag<sup>+</sup> Ion Exchange== | ||
| + | * The protocol from [[User:Melissa_Novy/Notebook/CHEM-572/2013/01/29|2013/01/29]] was followed. However, the solution will be stirred for 1 week, instead of 24 hours. | ||
| + | * Theoretical mass Laponite: 1.5 g | ||
| + | ** Actual mass Laponite: 1.49711 g | ||
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| + | * Theoretical mass AgNO<sub>3</sub>: 0.000524 g | ||
| + | ** Actual mass AgNO<sub>3</sub>: 0.00622 g | ||
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| + | * Observations: The solution became opaque and white in color after all components were added. | ||
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Revision as of 14:31, 5 February 2013
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Objectives
CalculationsMW AgNO3: 169.87 g/mol MW Ag+: 107.86 g/mol CEC Laponite: 55 meqv/100 g 1.5 g LMT × (55 meqv/100 g LMT) × (1 mol Ag+/1000 meqv) × (107.86 g Ag+/1 mol Ag+) × (1 mol Ag+/1 mol AgNO3) × (1 mol AgNO3/169.87 g AgNO3) × 100% = 0.000524 g AgNO3 Laponite-Ag+ Ion Exchange
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