User:Mary Mendoza/Notebook/CHEM 581: Experimental Chemistry I/2014/10/03: Difference between revisions

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==Ion Exchanged Clay==
==Ion Exchanged Clay==
* Films cast on lab period [User:Mary Mendoza/Notebook/CHEM 581: Experimental Chemistry I/2014/09/26|9/26/2014] were observed to be foamy. In addition, granules of the exchanged clay compounds were observed. The film is not homogenized and clay was not thoroughly dispersed.
* Films cast on lab period [[User:Mary Mendoza/Notebook/CHEM 581: Experimental Chemistry I/2014/09/26|9/26/2014]] were observed to be foamy. In addition, granules of the exchanged clay compounds were observed. The film is not homogenized and clay was not thoroughly dispersed.
* Second trial in exchanging the ions in the clay made use of choline chloride and tributylhexadecylphosphonium bromide.
* Second trial in exchanging the ions in the clay made use of choline chloride and tributylhexadecylphosphonium bromide.
* The weights of each compound were written on the vial as depicted below the attached picture.
* The weights of each compound were written on the vial as depicted below the attached picture.
* The exchanged clay were prepared using [[User:Matt_Hartings/Notebook/AU_Biomaterials_Design_Lab/2014/09/10| Dr. Hartings' procedure]].
* The exchanged clay were prepared using [[User:Matt_Hartings/Notebook/AU_Biomaterials_Design_Lab/2014/09/10| Dr. Hartings' procedure]].


[[Image:IMG 3120.JPG|thumb|center|800x600px]]


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Revision as of 19:17, 10 December 2014

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Completion of Malachite Green Diffusion through PVA-clay film

  • At 2294 minutes, the absorbance for the last measurement was taken.
  • Data analysis was initiated to find the diffusion coefficient for the malachite green.

Film Syntheses

  • The following weights of the materials were used for the syntheses of films; protocol may be viewed here.
    • 0.11151g clay + 1.00047g PVA
    • 0.11463g clay + 1.00168g PVA
    • 1.00733g PVA

Ion Exchanged Clay

  • Films cast on lab period 9/26/2014 were observed to be foamy. In addition, granules of the exchanged clay compounds were observed. The film is not homogenized and clay was not thoroughly dispersed.
  • Second trial in exchanging the ions in the clay made use of choline chloride and tributylhexadecylphosphonium bromide.
  • The weights of each compound were written on the vial as depicted below the attached picture.
  • The exchanged clay were prepared using Dr. Hartings' procedure.