User:Madeleine Y. Bee/Notebook/CHEM-581 Experimental Chemistry/2014/10/22: Difference between revisions
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|style="background-color: #EEE"|[[Image:BDLlogo_notext_lr.png|128px]]<span style="font-size:22px;"> CHEM 581: Experimental Chemistry</span> | |style="background-color: #EEE"|[[Image:BDLlogo_notext_lr.png|128px]]<span style="font-size:22px;"> CHEM 581: Experimental Chemistry</span> | ||
|style="background-color: #F2F2F2" align="center"| | |style="background-color: #F2F2F2" align="center"|[[File:Report.png|frameless|link={{#sub:{{FULLPAGENAME}}|0|-11}}]][[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|[[File:Resultset_previous.png|frameless|link={{#lnpreventry:{{FULLPAGENAME}}}}]][[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]] }}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]][[File:Resultset_next.png|frameless|link={{#lnnextentry:{{FULLPAGENAME}}}}]]}} | ||
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===Procedures=== | ===Procedures=== | ||
====Finish Film Synthesis from 10/17==== | ====Finish Film Synthesis from 10/17==== | ||
====Film Masses for Density Calculations==== | ====Film Masses for Density Calculations==== | ||
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| align="center" style="background:#f0f0f0;"|'''Initial Mass''' | | align="center" style="background:#f0f0f0;"|'''Initial Mass''' | ||
| align="center" style="background:#f0f0f0;"|'''Dried Mass''' | | align="center" style="background:#f0f0f0;"|'''Dried Mass''' | ||
| align="center" style="background:#f0f0f0;"|'''Displaced Volume''' | |||
|- | |||
| PVA film|| 0.0278g || 0.0102g || 0.048mL | |||
|- | |||
| || 0.0255g || 0.0129g || | |||
|- | |||
| || 0.0265g || 0.0089g || 0.114mL | |||
|- | |||
| PVA-Clay film|| 0.0122g || 0.0067g || | |||
|- | |||
| || 0.0177g ||0.0102g || | |||
|- | |||
| || 0.0307g || 0.0145g || | |||
|} | |||
====BPA Sample Prep==== | |||
*10ppm BPA stock solution made by James and Eleni | |||
**10.4 mg BPA was dissolved in 5 mL of methanol, then diluted to 1 L with water | |||
*Two measurements (for GC-MS and HPLC) for each time slot: | |||
**10/22 5 min | |||
**10/22 15 min | |||
**10/22 30 min | |||
**10/22 60 min | |||
**10/22 120 min | |||
**10/22 afternoon | |||
**10/23 morning | |||
**10/23 afternoon | |||
**10/24 | |||
*Using PVA-Clay film | |||
{| {{table}} | |||
| align="center" style="background:#f0f0f0;"|'''Sample''' | |||
| align="center" style="background:#f0f0f0;"|'''Vial''' | |||
| align="center" style="background:#f0f0f0;"|'''Mass of Empty Vial (g)''' | |||
| align="center" style="background:#f0f0f0;"|'''Mass of Film + Vial (g)''' | |||
| align="center" style="background:#f0f0f0;"|'''Film Mass (g)''' | |||
|- | |||
| GC-MS || 10/22 5 min|| 13.0961 || 13.2417 || 0.1456 | |||
|- | |||
| || 10/22 15 min || 13.0637 || 13.1933 || 0.1296 | |||
|- | |||
| || 10/22 30 min || 13.0670 || 13.2869 || 0.2199 | |||
|- | |||
| || 10/22 60 min|| 13.0693 || 13.2071 || 0.1378 | |||
|- | |||
| || 10/22 120 min || 13.0977 || 13.3447 || 0.2470 | |||
|- | |||
| || 10/22 afternoon || 13.0519 || 13.2186 || 0.1667 | |||
|- | |||
| || 10/23 morning || 13.0361 || 13.1181 || 0.0820 | |||
|- | |||
| || 10/23 afternoon || 13.0016 || 13.1543 || 0.1527 | |||
|- | |||
| || 10/24 || 13.0731 || 13.2344 || 0.1613 | |||
|- | |||
| HPLC || 10/22 5 min|| 13.0393 || 13.2924 || 0.2531 | |||
|- | |||
| || 10/22 15 min || 13.0428 || 13.1814 || 0.1386 | |||
|- | |||
| || 10/22 30 min || 13.0879 || 13.3509 || 0.2630 | |||
|- | |- | ||
| | | || 10/22 60 min|| 13.1562 || 13.3389 || 0.1827 | ||
|- | |- | ||
| | | || 10/22 120 min || 13.1078 || 13.2840 || 0.1762 | ||
|- | |- | ||
| | | || 10/22 afternoon || 13.0813 || 13.1784 || 0.0971 | ||
|- | |- | ||
| | | || 10/23 morning || 13.1008 || 13.2877 || 0.1869 | ||
|- | |- | ||
| | | || 10/23 afternoon || 13.0785 || 13.2066 || 0.1281 | ||
|- | |- | ||
| | | || 10/24 || 13.0254 || 13.1791 || 0.1537 | ||
|} | |} | ||
Latest revision as of 00:27, 27 September 2017
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October 22, 2014ProceduresFinish Film Synthesis from 10/17Film Masses for Density Calculations
BPA Sample Prep
Data |