User:Madeleine Y. Bee/Notebook/CHEM-581 Experimental Chemistry/2014/09/12: Difference between revisions
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===Procedures=== | ===Procedures=== | ||
====New Exfoliated Clay Film Synthesis==== | ====New Exfoliated Clay Film Synthesis==== | ||
#Determine how much 4% exfoliated NaMT needed for 10% clay solution | |||
#Add ~1g PVA | |||
#Stir the solution with constant heating at 75C until the polymer is dissolved and the clay is dispersed (~15 minutes) | |||
#Cool the solution to room temperature | |||
#Add 0.5mL 0.8 wt% glutaraldehyde | |||
#Stir for an additional 3 minutes to ensure homogeneity | |||
#Pour solution into teflon dish to dry | |||
====Powder X-ray Diffraction Measurements==== | ====Powder X-ray Diffraction Measurements==== | ||
Revision as of 04:36, 12 September 2014
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September 12, 2014ProceduresNew Exfoliated Clay Film Synthesis
Powder X-ray Diffraction Measurements | |
