User:Madeleine Y. Bee/Notebook/CHEM-581 Experimental Chemistry/2014/09/03: Difference between revisions

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[[User:Matt Hartings|Matt Hartings]] You need to update these graphs. The axes are too cramped, i.e. change your number formatting. Also, the graphs need to go from 4000cm-1 to 400cm-1




Revision as of 08:27, 12 September 2014

DSC & FTIR Measurements <html><img src="/images/9/94/Report.png" border="0" /></html> Main project page
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September 3, 2014

Procedures

Completing Film Synthesis

Continued from Friday, 8/29/2014<br.> Procedure detailed by Dr Hartings

  • Stir in Sodium Sulfate, 1% HCl, and Sodium Bicarbonate solutions

Beginning New Film Synthesis

Procedure detailed by Dr Hartings

  • Polymer-10% Clay Film
    • 1.0012 g PVA and 0.1120 g sodium montmorillonite (~1g PVA and ~.1g NaM)
  • Polymer Film
    • 1.0077 g PVA (~1g)

Differential Scanning Calorimetry Measurements

  • Polymer-10% Clay Film in 2 ppm MG
    • Pan and lid mass: 0.05289 g
    • Film mass: 0.00406 g
  • Polymer-10% Clay Film in 8 ppm MG
    • Pan and lid mass: 0.05226 g
    • Film mass: 0.00549 g
  • Polymer-10% Clay Film in 80 ppm MG
    • Pan and lid mass: 0.05297 g
    • Film mass: 0.00338 g
  • Polymer-10% Clay Film in 200 ppm MG
    • Pan and lid mass: 0.05253 g
    • Film mass: 0.00346 g
  • Polymer Film in 2 ppm MG
    • Pan and lid mass: 0.05299 g
    • Film mass: 0.0388 g
  • Polymer Film in 8 ppm MG
    • Pan and lid mass: 0.05225 g
    • Film mass: 0.00349 g
  • Polymer Film in 80 ppm MG
    • Pan and lid mass: 0.04741 g
    • Film mass: 0.00393 g
  • Polymer Film in 200 ppm MG
    • Pan and lid mass: 0.05242 g
    • Film mass: 0.00349 g
  • Polymer-10% Clay Film
    • Pan and lid mass: 0.05261 g
    • Film mass: 0.00442 g
  • Polymer Film
    • Pan and lid mass: 0.05213 g
    • Film mass: 0.00471 g

<br.>

FTIR: Total Attenuated Reflectance Measurements


Matt Hartings You need to update these graphs. The axes are too cramped, i.e. change your number formatting. Also, the graphs need to go from 4000cm-1 to 400cm-1




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