User:Khyra A. Neal/Notebook/Experimental Biological Chemistry II Notebook/2015/02/25: Difference between revisions
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(Autocreate 2015/02/25 Entry for User:Khyra_A._Neal/Notebook/Experimental_Biological_Chemistry_II_Notebook) |
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== | ==February 25, 2015== | ||
==Objective== | |||
# Analyze reaction mixture from previous day | |||
==Description== | |||
# The oxidation reaction that ran the [http://openwetware.org/wiki/User:Khyra_A._Neal/Notebook/Experimental_Biological_Chemistry_II_Notebook/2015/02/24 previous] was filtered then dissolved in ethyl acetate to separate the nanoparticles from the products. | |||
#* The mixture was centrifuged for 2 minutes to recover the nanoparticles | |||
#After centrifuging, the mixture was transferred to a 20 mL sample vial | |||
# 10 drops of the solution was dried on a watch glass | |||
# After drying, CDCl<sub>3</sub> was added to the watch glass and the solution was transferred to a NMR tube for proton analysis | |||
==Data== | |||
**INSERT NMR SPECTRA** | |||
==Notes== | |||
The NMR data shows that benzhydrol did not fully convert to benzophenone. The spectrum shows 11 hydrogens and multiple split peaks. | |||
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Revision as of 21:02, 2 March 2015
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February 25, 2015Objective
Description
Data
NotesThe NMR data shows that benzhydrol did not fully convert to benzophenone. The spectrum shows 11 hydrogens and multiple split peaks. |