User:Khyra A. Neal/Notebook/Chem 571/2014/10/15: Difference between revisions
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==October 15, 2014== | ==October 15, 2014== | ||
===Tasklist=== | ===Tasklist=== | ||
==Electrophoresis== | |||
* Warm solutions for 5 minutes at 40°C that were prepared on [http://openwetware.org/wiki/User:Khyra_A._Neal/Notebook/Chem_571/2014/10/14 October 14, 2014] | * Warm solutions for 5 minutes at 40°C that were prepared on [http://openwetware.org/wiki/User:Khyra_A._Neal/Notebook/Chem_571/2014/10/14 October 14, 2014] | ||
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===Determination of Dialyzed KI Samples extracted on [http://openwetware.org/wiki/User:Khyra_A._Neal/Notebook/Chem_571/2014/10/08 October 14, 2014]=== | |||
==Determination of KI Concentration by Titration== | |||
[KI]= 0.0000493 mol KI / 0.001 L KI = '''49.3 mM KI''' | * Standardization: | ||
** AgNO<sub>3</sub> + NH<sub>4</sub>SCN → AgSCN + NH<sub>4</sub>NO<sub>3</sub> | |||
** KI + AgNO<sub>3</sub>(excess) → AgI (s) + AgNO<sub>3</sub> +KNO<sub>3</sub> | |||
*** Initial AgNO<sub>3</sub>: 0.075 M AgNO<sub>3</sub> x 0.002 L AgNO<sub>3</sub> = '''0.00015 mol AgNO<sub>3</sub>''' | |||
*** AgNO<sub>3</sub> (neutralized): 0.00968 M NH<sub>4</sub>SCN x 0.0104 L NH<sub>4</sub>SCN x (1 mol AgNO<sub>3</sub> / 1 mol NH<sub>4</sub>SCN ) = '''0.000100672 mol AgNO<sub>3</sub>''' | |||
*** Moles of KI: 0.00015 mol AgNO<sub>3</sub> <sub>initial</sub> - 0.000100672 mol AgNO<sub>3</sub> <sub>neutralized</sub> = '''0.0000493 mol KI''' | |||
*** [KI]= 0.0000493 mol KI / 0.001 L KI = '''49.3 mM KI''' | |||
'''NOTE''' The final concentration of NH<sub>4</sub>SCN was determined by titration standardization on [http://openwetware.org/wiki/User:Khyra_A._Neal/Notebook/Chem_571/2014/10/08 October 8, 2014] | '''NOTE''' The final concentration of NH<sub>4</sub>SCN was determined by titration standardization on [http://openwetware.org/wiki/User:Khyra_A._Neal/Notebook/Chem_571/2014/10/08 October 8, 2014] |
Revision as of 09:00, 21 October 2014
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October 15, 2014TasklistElectrophoresis
The original protocol for electrophoresis was written by Dr. Hartings
Determination of Dialyzed KI Samples extracted on October 14, 2014Determination of KI Concentration by Titration
NOTE The final concentration of NH4SCN was determined by titration standardization on October 8, 2014
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