User:Karlena L. Brown/Notebook/PVOH Research/2013/04/03: Difference between revisions
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Figure 1 - Microsphere 90:10 PVOH 146K 50% CEC NaMT w/ Bu<sub>3</sub>HdP<sup>+</sup> | Figure 1 - Microsphere 90:10 PVOH 146K 50% CEC NaMT w/ Bu<sub>3</sub>HdP<sup>+</sup> | ||
<br> | <br> | ||
[[Image:90 pva 146 50NaMT micros diffusion.jpg]] | [[Image:90 pva 146 50NaMT micros diffusion.jpg|400px]] | ||
<br> | <br> | ||
''***Fluorescence intensity maximum is 6.985'' | ''***Fluorescence intensity maximum is 6.985'' | ||
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Figure 2 - Microsphere 90:10 PVOH 146K 110% CEC Laponite w/ DMHXLBR | Figure 2 - Microsphere 90:10 PVOH 146K 110% CEC Laponite w/ DMHXLBR | ||
<br> | <br> | ||
[[Image:90 PVA 146 110LP micros diff.jpg]] | [[Image:90 PVA 146 110LP micros diff.jpg|400px]] | ||
<br> | <br> | ||
''***Fluorescence intensity maximum is 5.109'' | ''***Fluorescence intensity maximum is 5.109'' | ||
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Figure 3 - Microsphere 90:10 PVOH 146K NaMT | Figure 3 - Microsphere 90:10 PVOH 146K NaMT | ||
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[[Image:90 PVA 146 NaMT micros diff test.png]] | [[Image:90 PVA 146 NaMT micros diff test.png|400px]] | ||
<br> | <br> | ||
''***Fluorescence intensity maximum is 26.734'' | ''***Fluorescence intensity maximum is 26.734'' | ||
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Figure 4 - Microsphere 50:50 PVOH 146K NaMT | Figure 4 - Microsphere 50:50 PVOH 146K NaMT | ||
<br> | <br> | ||
[[Image:50 PVA 146 NaMT micros diff.png]] | [[Image:50 PVA 146 NaMT micros diff.png|400px]] | ||
''***Fluorescence intensity maximum is 17.'' | ''***Fluorescence intensity maximum is 17.'' | ||
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Figure 5 - Microsphere 50:50 PVOH 146K 50% CEC NaMT w/ Bu<sub>3</sub>HdP<sup>+</sup> | Figure 5 - Microsphere 50:50 PVOH 146K 50% CEC NaMT w/ Bu<sub>3</sub>HdP<sup>+</sup> | ||
<br> | <br> | ||
[[Image:50 PVA 146 50NaMT micros diff.png]] | [[Image:50 PVA 146 50NaMT micros diff.png|400px]] | ||
<br> | <br> | ||
''***Fluorescence intensity maximum is 11.661'' | ''***Fluorescence intensity maximum is 11.661'' | ||
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Figure 6 - Microsphere 50:50 PVOH 146K 110% CEC Laponite w/ DMHXLBR | Figure 6 - Microsphere 50:50 PVOH 146K 110% CEC Laponite w/ DMHXLBR | ||
<br> | <br> | ||
[[Image:50 PVA 146 110 LP.png]] | [[Image:50 PVA 146 110 LP.png|400px]] | ||
<br> | <br> | ||
''***Fluorescence intensity maximum is 137.319'' | ''***Fluorescence intensity maximum is 137.319'' |
Revision as of 15:19, 14 April 2013
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OBJECTIVES
DSC Results for Dry Clay SamplesDSC Analysis: Mixed MicrospheresDSC preparation and protocol involving instrumentation and usage can be found on 9/17/12 entry.
# Equilibrate sample at ~ -40°C # Ramp sample temperature up from 20-240°C # Ramp sample temperature down from 20-(-40°C) # Repeat segment #2 again Fluorescence Analysis: Diffusion Testing 2RECALL DIFFUSION TESTING PROTOCOL ON 2/15/13
# Microsphere 90:10 PVOH 146K 50% CEC NaMT w/ Bu3HdP+ # Microsphere 90:10 PVOH 146K 110% CEC Laponite w/ DMHXLBR # Microsphere 90:10 PVOH 146K NaMT # Microsphere 50:50 PVOH 146K NaMT # Microsphere 50:50 PVOH 146K 50% CEC NaMT w/ Bu3HdP+ # Microsphere 50:50 PVOH 146K 110% CEC Laponite w/ DMHXLBR
# Excitation: 480nm # Emission Range: 500-650nm # Excitation Slit Width: 10 # Emission Slit Width: 10 # Scan Speed: 1200 Fluorescence Results & Spectrums
Notes
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