User:Karlena L. Brown/Notebook/PVOH Research/2013/03/20

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(OBJECTIVES)
Current revision (16:20, 24 March 2013) (view source)
(Notes)
 
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* Prepare more microsphere samples expanding upon new previous method developed (new modifications)
* Prepare more microsphere samples expanding upon new previous method developed (new modifications)
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==PVOH 146K & 130K Prepared Microsphere Samples & Dye Preparations 4==
+
==PVOH 146K Prepared Microsphere Samples & Dye Preparations 4==
'''RECALL MICROSPHERE PREPARATION PROTOCOL ON 2/20/13'''
'''RECALL MICROSPHERE PREPARATION PROTOCOL ON 2/20/13'''
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| 90:10||110% CEC NaMT w/ DMHXLBR||0.01070||0.09100||40||92||109
| 90:10||110% CEC NaMT w/ DMHXLBR||0.01070||0.09100||40||92||109
|}
|}
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==PVOH 130K Prepared Microsphere Samples & Dye Preparations==
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'''RECALL MICROSPHERE PREPARATION PROTOCOL ON 2/20/13'''
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'''1μM Rhodamine 6G Dye Concentration (90:10)'''
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  M<sub>1</sub>V<sub>1</sub> = M<sub>2</sub>V<sub>2</sub>
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  1μM (RG6)x 10mL = (92μM)V<sub>2</sub>    V<sub>2</sub> = 109μL
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 +
'''1μM Rhodamine 6G Dye Concentration (50:50)'''
 +
  M<sub>1</sub>V<sub>1</sub> = M<sub>2</sub>V<sub>2</sub>
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  1μM (RG6)x 10mL = (165μM)V<sub>2</sub>    V<sub>2</sub> = 61μL
{| {{table}}
{| {{table}}
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| 90:10||110% CEC NaMT w/ DMHXLBR||0.01090||0.09340||40||92||109
| 90:10||110% CEC NaMT w/ DMHXLBR||0.01090||0.09340||40||92||109
|}
|}
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==Notes==
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* Unfortunately, DSC samples were not taken before the Rhodamine 6G dye was added to each sample; therefore, these samples must be remade.
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Current revision

PVOH Research Main project page
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OBJECTIVES

  • Continue to clean, filter, and separate out the oil from the previously prepared microspheres on 2/22/13
  • Prepare more microsphere samples expanding upon new previous method developed (new modifications)

PVOH 146K Prepared Microsphere Samples & Dye Preparations 4

RECALL MICROSPHERE PREPARATION PROTOCOL ON 2/20/13

1μM Rhodamine 6G Dye Concentration (90:10)

  M1V1 = M2V2
  1μM (RG6)x 10mL = (92μM)V2    V2 = 109μL

1μM Rhodamine 6G Dye Concentration (50:50)

  M1V1 = M2V2
  1μM (RG6)x 10mL = (165μM)V2    V2 = 61μL
PVOH vs. Clay Ratio Clay Selection PVOH 146K Mass (g) Actual Clay Mass (g) H2O Added (mL) Dye Concentration (μM) Dye Amount Added (μL)
50:50110% CEC NaMT w/ DMHXLBR0.050100.051004016561
90:10110% CEC NaMT w/ DMHXLBR0.010700.091004092109

PVOH 130K Prepared Microsphere Samples & Dye Preparations

RECALL MICROSPHERE PREPARATION PROTOCOL ON 2/20/13

1μM Rhodamine 6G Dye Concentration (90:10)

  M1V1 = M2V2
  1μM (RG6)x 10mL = (92μM)V2    V2 = 109μL

1μM Rhodamine 6G Dye Concentration (50:50)

  M1V1 = M2V2
  1μM (RG6)x 10mL = (165μM)V2    V2 = 61μL
PVOH vs. Clay Ratio Clay Selection PVOH 130K Mass (g) Actual Clay Mass (g) H2O Added (mL) Dye Concentration (μM) Dye Amount Added (μL)
50:50110% CEC NaMT w/ DMHXLBR0.050700.051304016561
90:10110% CEC NaMT w/ DMHXLBR0.010900.093404092109

Notes

  • Unfortunately, DSC samples were not taken before the Rhodamine 6G dye was added to each sample; therefore, these samples must be remade.


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